二氧化铅电极的制备工艺
Preparation Technology of Lead Dioxide Electrode
摘 要
采用脉冲电流技术制备钛基二氧化铅电极, 研究了脉冲电流密度, 脉冲时间, 脉冲间隔等因素对钛基二氧化铅形貌以及电化学特性的影响。与直流电镀二氧化铅比较, 利用脉冲电镀制备的二氧化铅镀层更加致密, 电化学性能更加稳定。
脉冲电镀
电化学测试
PbO2
pulse plating
electrochemical test
Abstract
Lead dioxide coating was prepared on a Ti substrate by pulsed current technique. The effect of the pulsed current density, pulsed time and relaxation time on the morphology and electrochemical properties of the coating was studied by means of scanning electron microscopy and electrochemical testing. Compared with lead dioxide fabricated by common electroplate technique, lead dioxide prepared by pulsed current technique is more dense, has no hole, shows better corrosion resisting property and more stable electrochemical properties.
中图分类号 TG174.4
所属栏目 应用技术
基金项目 国家科技支撑计划项目(2012BAE06B06); 广西千亿元产业重大科技攻关项目(2012AA04018)
收稿日期 2012/7/25
修改稿日期
网络出版日期
作者单位点击查看
备注尹卫华, 助理工程师, 学士,
引用该论文: YIN Wei-hua,YANG Li-na,ZHOU Yu-gao,WEI Zhi-wei. Preparation Technology of Lead Dioxide Electrode[J]. Corrosion & Protection, 2013, 34(1): 71
共有人对该论文发表了看法，其中：
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】谢天, 王斌.二氧化铅电极制备方法综述[J].成都大学学报(自然科学版), 2003, 22(3):25-30.
【2】汪文兵, 龙晋明, 郭忠诚.钛基金属氧化物涂层电极研究进展[J].电镀与涂饰, 2006, 25(7):46-50.
【3】Jaeyoung Lee, Hamilton Varela, Sunghyun Uhm.Electrodeposition of PbO onto Au and Ti substrates[J].Electrochemistry Communications, 2000(2):646-652.
【4】Vatistas N, Cristofaro S.Lead dioxide coating obtained by pulsed current technique[J].Electrochemistry Communications, 2000(2):334-337.
【5】Shen P K, Wei X L.Morphologic study of electrochemically formed lead dioxide[J].Electrochimica Acta, 2003(48):1743-1747.
【2】汪文兵, 龙晋明, 郭忠诚.钛基金属氧化物涂层电极研究进展[J].电镀与涂饰, 2006, 25(7):46-50.
【3】Jaeyoung Lee, Hamilton Varela, Sunghyun Uhm.Electrodeposition of PbO onto Au and Ti substrates[J].Electrochemistry Communications, 2000(2):646-652.
【4】Vatistas N, Cristofaro S.Lead dioxide coating obtained by pulsed current technique[J].Electrochemistry Communications, 2000(2):334-337.
【5】Shen P K, Wei X L.Morphologic study of electrochemically formed lead dioxide[J].Electrochimica Acta, 2003(48):1743-1747.
相关信息
