Effect of Cu Contents on Microstructure and Creep Property of High Chromium Ferric Steels
摘 要
对含不同质量分数(0, 0.6%, 3%)铜的高铬铁素体钢在650 ℃和140 MPa条件下蠕变前后的组织和蠕变性能进行了研究。结果表明: 随着铜含量从0提高3%, 钢的蠕变断裂时间从1 172 h提高到1 620 h, 蠕变速率从2.2×10-9s-1降低到1.2×10-9s-1; 铜的添加有效抑制了对蠕变性能不利的高温δ铁素体相的形成; 添加3%铜的试验钢基体内弥散析出了大量尺寸为50~100 nm的富铜相, 有效抑制了位错的运动, 从而提高了该钢的蠕变抗力。
Abstract
The microstructure and creep property before and after creep of three high chromium ferric steels with 0wt%Cu, 0.6wt%Cu and 3wt%Cu were studied under the conditions of 650 ℃ and 140 MPa. The results show that the creep fracture time increasing from 1 172 h to 1 620 h and the creep rate decreased from 2.2×10-9 s-1 to 1.2×10-9 s-1 with the Cu content increasing from 0wt% to 3wt%. The addition of Cu effectively suppressed forming high temperature δ-ferrite phase adverse to the creep property.Numerous Cu-rich phases with the size of 50-100 nm dispersedly precipitated in the matrix of the tested steel with 3wt%Cu, which could effectively restrain the motion of dislocation and thus increase the creep resistance of the steel.
中图分类号 TG113
所属栏目 试验研究
基金项目
收稿日期 2011/5/4
修改稿日期 2011/11/18
网络出版日期
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备注沈喜训(1977-), 男, 上海人, 工程师, 博士。
引用该论文: SHEN Xi-xun,LIU Jun-liang,SHEN Wei. Effect of Cu Contents on Microstructure and Creep Property of High Chromium Ferric Steels[J]. Materials for mechancial engineering, 2012, 36(4): 12~16
沈喜训,刘俊亮,沈巍. 铜含量对高铬铁素体钢组织和蠕变性能的影响[J]. 机械工程材料, 2012, 36(4): 12~16
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参考文献
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【3】SAKAKIBARA M, MASUMOTO H, OGAWA T, et al. High strength 9Cr-0.5Mo-1.8W steel (NF616) tubes for boilers [J].Thermal and Nuclear Power, 1987, 38: 841-850.
【4】CERJAK H, LETOFSKY E, FEIGL G, et al. Materials for advanced power engineering [M].JLICH, Forschungszentrum: JLICH GMBH, 1998: 1211-1221.
【5】ISEDA A, SAWARAGI Y, KATO S, et al. Creep characterization, damage and life assessment[C]//Proc 5th Int Conf Creep of Materials.Ohio, USA: ASM Int Metal Park, 1992: 389-293.
【6】刘俊亮.一种新型高铬铁素体钢的蠕变特性及显微组织研究[J].机械工程材料, 2011, 35(2): 54-57.
【7】WANG Q J, TOSHIAKI T, HONG J, et al. Effect of Co addition on the microstructure and creep properties of 12%Cr heat-resistant steels[C]//Shanghai: Baosteel BAC 2008, 2008: 197-201.
【8】YAMADA K, IGARASHI M, MUNEKI S, et al. Effect of Co addition on microstructure in high Cr ferrtitic steels[J].ISIJ International, 2001, 43: 1438-1443.
【9】FROST H J, ASHBY M F. Deformation mechanism maps [M].Oxford: Pergamon Press, 1982.
【10】KU B S, YU J. Effects of Cu addition on the creep rupture properties of a 12% Cr steel [J].Script Mater, 2001, 45: 205-211.
【11】DIMMLERG, WEINERT P, KOZESCHNIK E, et al. Quantification of the Laves phase in advanced 9%-12% Cr steels using a standard SEM [J].Materials characterization, 2003, 51: 341-352.
【12】朱丽慧, 赵钦新, 顾海澄, 等.新型耐热钢T91 的蠕变断裂寿命估算[J].锅炉技术, 2002, 33(5): 24-27.
【13】HAMADA K, TUKUNO K, TOMITA Y. Effects of precipitate shape on high temperature strength of modified 9Cr-1Mo steels[J]. ISIJ International, 1995, 35: 86-91.
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