分散液液微萃取技术在气相色谱法测定农药残留量中的应用
Application of Dispersive Liquid-Liquid Micro-extraction to GC-Determination of Residual Amounts of Pesticides
摘 要
介绍了分散液液微萃取(DLLME)技术的基本原理和萃取过程,介绍了萃取剂、分散剂、萃取时间、溶液的pH和离子强度等因素对萃取效果的影响;综述了DLLME与气相色谱法相结合在农药残留分析中的应用(引用文献55篇)。
气相色谱
农药
Dispersive liquid-liquid micro-extraction
GC
Pesticides
Abstract
A review on the progress of application of dispersive liquid-liquid micro-extraction (DLLME) to gas chromatographic determination of residual amounts of pesticides was given in this paper, relating especially to the topics on the principle and procedure of extraction, the influential factors of extraction, including extraction solvent, dispersing agents, extraction time, values of pH and ionic strength (55 ref. cited).
中图分类号 O652.62
所属栏目 综述
基金项目 国家自然科学基金项目(20805011)资助
收稿日期 2012/6/23
修改稿日期
网络出版日期
作者单位点击查看
联系人作者崔淑敏(wangwp@zjnu.cn)
备注崔淑敏(1987-),女,安徽蚌埠人,硕士研究生,研究方向为色谱分析及样品前处理。
引用该论文: CUI Shu-min,WANG Wei-ping,MIAO Ji-gen,CHEN Jian-rong. Application of Dispersive Liquid-Liquid Micro-extraction to GC-Determination of Residual Amounts of Pesticides[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2013, 49(8): 1011～1016
崔淑敏,王卫平,缪吉根,陈建荣. 分散液液微萃取技术在气相色谱法测定农药残留量中的应用[J]. 理化检验－化学分册, 2013, 49(8): 1011～1016
被引情况:
【1】彭淑香,张丽君,张占恩,徐知雄, "分散液相微萃取-石墨炉原子吸收光谱法测定水样中痕量铅",理化检验－化学分册 51, 1422-1425(2015)
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【4】胡媛,刘文民,周艳明,等.色谱［J］, 2006,24(3):290-293.
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【7】金竹萍.山西化工［J］, 2007,27(2):42-46.
【8】房贤文,谭培功.分析试验室［J］, 2007,26(7):100-103.
【9】邵焰,张丽君,张占恩.分析化学［J］, 2011,39(11):1753-1757.
【10】沈宋利,卢珩俊,魏超,等.理化检验-化学分册［J］, 2013,49(1):63-65.
【11】REZAEE M, ASSADI Y, HOSSEINI M-R M, et al. J Chromatogr A［J］, 2006,1116:1-9.
【12】HOSSEINI M H, REZAEE M, AKBARIAN S, et al. Anal Chim Acta［J］, 2013,762:54-60.
【13】REZAEE M, YAMINI Y, MORADI M, et al. J Supercritical Fluids［J］, 2010,55:161-168.
【14】FATTAHI N, ASSADI Y, HOSSEINI M-R M, et al. J Chromatogr A［J］, 2007,1157:23-29.
【15】LI Xiao-yi, XUE Ai-fang, CHEN Hao, et al. J Chromatogr A［J］, 2013,1280:9-15.
【16】CHAO Yu-ying, TU Yi-ming, JIAN Zhi-xuan, et al. J Chromatogr A［J］, 2013,1271:41-49.
【17】FATTAHI N, SAMADI S, ASSADI Y, et al. J Chromatogr A［J］, 2007,1169:63-69.
【18】LANA N B, BERTON P, COVACI A, et al. J Chromatogr A［J］, 2013,1258:12-21.
【19】ZHANG Yu-feng, LEE H K. J Chromatogr A［J］, 2013,1274:28-35.
【20】JIA Shao-dong, RYU Y, KWON S W, et al. J Chromatogr A［J］, 2013,1282:1-10.
【21】YOUSEFI S M, SHEMIRANI F. J Hazard Mater［J］, 2013,254/255:134-140.
【22】MOHAMMADI S Z, AFZALI D, BAGHELANI Y M. Anal Chim Acta［J］, 2009,653:173-177.
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【25】葛娜,刘晓茂,李学民,等.分析测试学报［J］, 2011,30(12):1351-1355.
【26】马燕玲,陈令新,丁养军,等.色谱［J］, 2013,31(2):155-161.
【27】毛秀红,郏征伟,苗水,等.中成药［J］, 2010,32(3):454-459.
【28】田宏哲,赵瑛博,周艳明.食品科学［J］, 2011,32(2):187-190.
【29】韩康,张衡,翟学良.食品科技［J］, 2011,36(2):293-296.
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【35】赵文婷,杨中华,魏朝俊,等.农业环境科学学报［J］, 2010,29(9):1840-1844.
【36】SAMADI S, SERESHTI H, ASSADI Y. J Chromatogr A［J］, 2012,1219:61-65.
【37】CORTADA C, VIDAL L, PASTOR R, et al. Anal Chim Acta［J］, 2009,649:218-221.
【38】TSAI W C, HUANG S D. J Chromatogr A［J］, 2009,1216:5171-5175.
【39】LEONG M I, HUANG S D. J Chromatogr A［J］, 2009,1216:7645-7650.
【40】ZACHARIS C K, ROTSIAS I, ZACHARIADIS P G, et al. Food Chem［J］, 2012,134:1665-1672.
【41】臧晓欢,王春,高书涛,等.分析化学［J］, 2008,36(6):765-769.
【42】DU Jing-jing, YAN Hong-yuan, SHE Dan-dan, et al. Talanta［J］, 2010,82:698-703.
【43】张晓赟,张丽君,张占恩.苏州科技学院学报［J］, 2011,24(4):4-8.
【44】李贤波,赵嫚,李胜清,等.色谱［J］, 2012,30(9):926-930.
【45】CHEN Hao, CHEN Rui-wen, LI Sheng-qing, et al. J Chromatogr A［J］, 2010,1217:1244-1248.
【46】NAGARAJU D, HUANG S D. J Chromatogr A［J］, 2007,1161:89-97.
【47】SANAGI M M, ABBAS H H, IBRAHIM W A W, et al. Food Chem［J］, 2012,133:557-562.
【48】ZHAO Ru-song, DIAO Chun-peng, WANG Xia, et al. Anal Bioanal Chem［J］, 2008,391:2915-2921.
【49】ZHAO Ru-song, DIAO Chun-peng, CHEN Qing-feng, et al. J Sep Sci［J］, 2009,32:1069-1074.
【50】READMAN J W, ALBANIS T A, BARCEL D, et al. Mar Pollut Bull ［J］, 1997,34(4):259-263.
【51】周欣,臧晓欢,王东跃,等.分析化学［J］, 2009,37(1):41-45.
【52】CUNHA S C, FERNANDES J O, OLIVEIRA M B, et al. J Chromatogr A［J］, 2009,1216:8835-8844.
【53】MONTES R, RODRGUEZ I, RAMIL M, et al. J Chromatogr A［J］, 2009,1216:5459-5466.
【54】RODRGUEZ-CABO T, RODRGUEZ I, RAMIL M, et al. J Chromatogr A［J］, 2011,1218:6603-6611.
【55】MELO A, CUNHA S C, MANSILHA C, et al. Food Chem［J］, 2012,135:1071-1077.
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