电导滴定法同时测定羧甲基壳聚糖的取代度、脱乙酰度和-COONa分布系数
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Abstract
中图分类号 O655.22 O657.11
所属栏目 知识与经验
基金项目 山东省自然科学基金(ZR2012CQ015);青岛农业大学大学生科技创新基金(2013191);青岛农业大学高层次人才科研基金(631008)
收稿日期 2014/5/27
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引用该论文: 孔祥平,张保华,钟鑫,郇聪聪,于丹丹,王娟. [J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2015, 51(5): 697～700
孔祥平,张保华,钟鑫,郇聪聪,于丹丹,王娟. 电导滴定法同时测定羧甲基壳聚糖的取代度、脱乙酰度和-COONa分布系数[J]. 理化检验－化学分册, 2015, 51(5): 697～700
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参考文献
【1】UPADHYAYA L,SINGH J,AGARWAL V,et al.Biomedical applications of carboxymethyl chitosans[J].Carbohydrate Polymers,2013,91(1):452-466.
【2】KONG Xiang-ping.Simultaneous determination of degree of deacetylation,degree of substitution and distribution fraction of -COONa in carboxymethyl chitosan by potentiometric titration[J].Carbohydrate Polymers,2012,88(1):336-341.
【3】刘敬兰,陈连文,何书美.顶空气相色谱法测定羧甲基壳聚糖中氯乙酸残留量[J].理化检验-化学分册,2012,48(2):144-146.
【4】陈凌云,杜予民.羧甲基壳聚糖的取代度及保湿性[J].应用化学,2001,18(1):5-8.
【5】贺君,司玫,韩宝芹,等.羧甲基壳聚糖的化学结构表征[J].中国海洋药物,2002(2):26-27.
【6】GE Hua-cai,LUO Deng-ke.Preparation of carboxymethyl chitosan in aqueous solution under microwave irradiation[J].Carbohydrate Research,2005,340(7):1351-1356.
【7】SUN Sheng-ling,WANG Ai-qin.Adsorption kinetics of Cu(Ⅱ) ions using N,O-carboxymethyl-chitosan[J].Journal of Hazardous Materials,2006,131(1/3):103-111.
【8】XUE Xu-ting,LI Ling,HE Jin-xin.The performances of carboxymethyl chitosan in wash-off reactive dyeings[J].Carbohydrate Polymers,2009,75(2):203-207.
【9】SONG Qing-ping,ZHANG Ze,GAO Jian-gang,et al.Synthesis and property studies of N-carboxymethyl chitosan[J].Journal of Applied Polymer Science,2011,119(6):3282-3285.
【10】MUZZARELLI R A A,TANFANI F,EMANUELLI M,et al.N-(carboxymethylidene) chitosans and N-(carboxymethyl) chitosans: novel chelating polyampholytes obtained from chitosan glyoxylate[J].Carbohydrate Research,1982,107(2):199-214.
【11】刘长霞,陈国华,晋治涛,等.N,O-羧甲基壳聚糖羧化度计算式的修正[J].北京化工大学学报,2004,31(2):14-17.
【12】顾月姝.基础化学实验(Ⅲ)-物理化学实验[M].北京:化学工业出版社,2006.
【13】ZAMANI A,HENRIKSSON D,TAHERZADEH,M J.A new foaming technique for production of superabsorbents from carboxymethyl chitosan[J].Carbohydrate Polymers,2010,80(4):1091-1101.
【14】VAGHANI S S,PATEL M M,SATISH C S.Synthesis and characterization of pH-sensitive hydrogel composed of carboxymethyl chitosan for colon targeted delivery of ornidazole[J].Carbohydrate Research,2012,347(1):76-82.
【15】LUO Yang-chao,TENG Zi,WANG Xiang-an,et al.Development of carboxymethyl chitosan hydrogel beads in alcohol-aqueous binary solvent for nutrient delivery applications[J].Food Hydrocolloids,2013,31(2):332-339.
【16】SC/T 3403-2004甲壳质与壳聚糖[S].
【17】GB 5009.3-2010食品安全国家标准-食品中水分的测定[S].
【18】孔祥平.红外光谱法测定壳聚糖脱乙酰度[J].应用化工,2012,41(8):1458-1461.
【2】KONG Xiang-ping.Simultaneous determination of degree of deacetylation,degree of substitution and distribution fraction of -COONa in carboxymethyl chitosan by potentiometric titration[J].Carbohydrate Polymers,2012,88(1):336-341.
【3】刘敬兰,陈连文,何书美.顶空气相色谱法测定羧甲基壳聚糖中氯乙酸残留量[J].理化检验-化学分册,2012,48(2):144-146.
【4】陈凌云,杜予民.羧甲基壳聚糖的取代度及保湿性[J].应用化学,2001,18(1):5-8.
【5】贺君,司玫,韩宝芹,等.羧甲基壳聚糖的化学结构表征[J].中国海洋药物,2002(2):26-27.
【6】GE Hua-cai,LUO Deng-ke.Preparation of carboxymethyl chitosan in aqueous solution under microwave irradiation[J].Carbohydrate Research,2005,340(7):1351-1356.
【7】SUN Sheng-ling,WANG Ai-qin.Adsorption kinetics of Cu(Ⅱ) ions using N,O-carboxymethyl-chitosan[J].Journal of Hazardous Materials,2006,131(1/3):103-111.
【8】XUE Xu-ting,LI Ling,HE Jin-xin.The performances of carboxymethyl chitosan in wash-off reactive dyeings[J].Carbohydrate Polymers,2009,75(2):203-207.
【9】SONG Qing-ping,ZHANG Ze,GAO Jian-gang,et al.Synthesis and property studies of N-carboxymethyl chitosan[J].Journal of Applied Polymer Science,2011,119(6):3282-3285.
【10】MUZZARELLI R A A,TANFANI F,EMANUELLI M,et al.N-(carboxymethylidene) chitosans and N-(carboxymethyl) chitosans: novel chelating polyampholytes obtained from chitosan glyoxylate[J].Carbohydrate Research,1982,107(2):199-214.
【11】刘长霞,陈国华,晋治涛,等.N,O-羧甲基壳聚糖羧化度计算式的修正[J].北京化工大学学报,2004,31(2):14-17.
【12】顾月姝.基础化学实验(Ⅲ)-物理化学实验[M].北京:化学工业出版社,2006.
【13】ZAMANI A,HENRIKSSON D,TAHERZADEH,M J.A new foaming technique for production of superabsorbents from carboxymethyl chitosan[J].Carbohydrate Polymers,2010,80(4):1091-1101.
【14】VAGHANI S S,PATEL M M,SATISH C S.Synthesis and characterization of pH-sensitive hydrogel composed of carboxymethyl chitosan for colon targeted delivery of ornidazole[J].Carbohydrate Research,2012,347(1):76-82.
【15】LUO Yang-chao,TENG Zi,WANG Xiang-an,et al.Development of carboxymethyl chitosan hydrogel beads in alcohol-aqueous binary solvent for nutrient delivery applications[J].Food Hydrocolloids,2013,31(2):332-339.
【16】SC/T 3403-2004甲壳质与壳聚糖[S].
【17】GB 5009.3-2010食品安全国家标准-食品中水分的测定[S].
【18】孔祥平.红外光谱法测定壳聚糖脱乙酰度[J].应用化工,2012,41(8):1458-1461.
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