蒸发冷凝法制备纳米粉体的研究进展
Progress in Research on Preparation of Nano-powder by Evaporation-condensation Method
摘 要
蒸发冷凝(IGC)法是纳米粉体制备的主要物理方法之一,可成功应用于金属、合金、金属氧化物等多种类型纳米粉体的制备;制备装置容易实现,可采用多种加热方式,如电阻加热法、等离子喷射加热法、感应加热法、电子束加热法、激光加热法等;目前关于制备工艺的研究主要集中在对影响纳米粉体粒径的工艺参数的研究和提高纳米粉体产率的研究上,而粉体粒径的影响因素多、产率难以明显提高也一直是制约该法发展的瓶颈;对采用该法制备的纳米粉体的性能研究表明,蒸发冷凝法制备的纳米粉体具有良好的力学性能、磁性能和光学特性.
纳米粉体
制备工艺
evaporation-condensation method
nano-powder
preparing technology
Abstract
Evaporation-condensation method has been a classical method to prepare nano-powders for a long time,and it is still a main physical method to prepare nano-powders today.The categories of nano-powders of metal,alloy and metallic oxide which can be prepared by evaporation-condensation method are recommended.Heating modes and their characteristics are introduced,including ohmic-resistance heating,plasma arc heating,induction heating,electron beam heating,laser heating,and so on.The present situation of research on preparing technology and property of nano-powders prepared by the method is summarized.The present research on preparing process is mainly focused on technological parameters which influence nano-powders diameter,and approaches to raise nano-powders yield rate.The nano-powders prepared by evaporation-condensation method have superior mechanical,magnetic and optical properties.
中图分类号 TQ029
所属栏目
基金项目 国家863计划资助项目(2002AA302608);中国矿业大学青年科研基金资助项目(E200410)
收稿日期 2007/4/4
修改稿日期 2007/6/7
网络出版日期
作者单位点击查看
备注鲍久圣(1979-),男,安徽桐城人,助教,博士研究生.
引用该论文: BAO Jiu-sheng,YIN Yan,LIU Tong-gang,YANG Zhi-yi. Progress in Research on Preparation of Nano-powder by Evaporation-condensation Method[J]. Materials for mechancial engineering, 2008, 32(2): 4～7
鲍久圣,阴妍,刘同冈,杨志伊. 蒸发冷凝法制备纳米粉体的研究进展[J]. 机械工程材料, 2008, 32(2): 4～7
共有人对该论文发表了看法，其中：
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】杨志伊.纳米科技[M].北京:机械工业出版社,2004:62-69.
【2】徐存英,王真,洪品杰.纳米粉体材料的制备[J].云南民族学院学报,1998,7(1):65-66.
【3】Takaki S,Yatsuya S.Nanoparticle produced by sputtering[C]//14th International Congress on Electron Microscopy.Cancun,Mexico:[s.n] 1998:469-470.
【4】杜芳林,崔作林,张志锟,等.纳米铜的制备、结构及催化性能[J].分子催化,1997,18(3):46-48.
【5】魏胜,王朝阳,黄勇,等.蒸发冷凝法制备纳米Al粉及其热反应特性研究[J].原子能科学技术,2002,36(4):367-370.
【6】胡军辉,吴润,黄为,等.激光感应复合加热蒸发冷凝法制备超微锌粉[J].激光技术,2000,24(2):100-101.
【7】魏智强,马军,冯旺军,等.等离子体制备银纳米粉末的研究[J].贵金属,2004,25(3):29-32.
【8】鲍久圣,刘同冈,杨志伊,等.蒸发冷凝法制备纳米粉体实验装置的研制[J].机电产品开发与创新,2004,17(5):18-19.
【9】刘同冈,鲍久圣,杨志伊.直流钨电弧法制备碳包覆铁纳米微粒的研究[J].中国矿业大学学报,2007,36(2):201-204.
【10】Yatsuya S.Growth of fullerene nanoparticles prepared by the gas-evaporation technique[J].Journal of Materials Science,1998,33(24):5843-5847.
【11】任瑞铭.纳米粉体材料制备技术[J].大连铁道学院学报,1999,20(3):69-72.
【12】陆必志,陈振兴,黄巧萍,等.纳米片状铝粉的制备及其发展动态[J].粉末冶金工业,2004,14(2):41-44.
【13】黄开金,谢长生,许德胜.激光蒸发冷凝法制备纳米颗粒的研究现状[J].激光技术,2004,28(1):5-11.
【14】陆必志,陈振兴.蒸发-冷凝法制备超细鳞片状锌粉[J].粉末冶金工业,2005,15(2):5-8.
【15】Champion,Yannick.Evaporation and condensation for metallic nanopowders[J].Annales de Chimie:Science des Materiaux,2006,31(3):281-29.
【16】Yan Hongge,Li Yunong,Chen Qing.Powder preparation with evaporation and condensation method[J].Journal of Hunan University Natural Sciences,2005,32(2):85-89.
【17】钟胜,戴永年.真空蒸发冷凝制备超细锌粉的研究[J].昆明理工大学学报,1998,23(3):48-52.
【18】陈允鸿,姜玉梅,朱骏,等.FeNi合金超细微粒的蒸发冷凝法制备及其微结构[J].南京大学学报,1994,30(4):600-605.
【19】陈允鸿,姜玉梅.蒸发冷凝法中气体压强和蒸发温度对粒子大小的影响[J].功能材料,1994,25(5):418-420.
【20】曹立宏,傅磊,樊友三.直流电弧等离子体制备TiN纳米粉末的研究[J].硅酸盐学报,1997,25(1):106-109.
【21】Singh,Yogendra.Approaches to increasing yield in evaporation/condensation nanoparticle generation[J].Journal of Aerosol Science,2002,33(9):1309-1325.
【22】鲍久圣,刘同冈,杨志伊,等.蒸发冷凝法制备纳米粉体反应容器中的温度场研究[J].机械科学与技术,2006,25(11):1334-1337.
【23】Yokoyama,Saito,Katsuyoshi.Evaporation rate of molten iron in Ar+O2 gas stream and characteristics of condensed particles[J].Journal of the Japan Institute of Metals,1995,59(10):1030-1035.
【24】陈允鸿,陈庆琉,邓桂昌,等.Fe-29wt%Ni合金超细微粒的压力效应[J].应用科学学报,1996,14(4):427-430.
【25】陈允鸿,朱骏,王锦辉,等.Fe-47wt%Ni纳米晶粉芯磁谱及其压力效应[J].功能材料,1997,28(6):655-657.
【26】夏辉,谢长生,胡军辉.表面钝化处理对纳米Zn粉抗氧化性能的影响[J].金属热处理学报,2000,21(3):17-20.
【27】苏眆,谢斌,陈允鸿.坡莫合金纳米粉的恒导磁性及其磁导率的压力、频率特性[J].高压物理学报,1995,9(4):247-255.
【28】朱骏,陈允鸿,王锦辉,等.退火对Fe-47%wtNi合金超细微粒压结体高频特性的影响[J].功能材料,1997,28(4):441-443.
【29】Champion Y,Bonnentien J-L,Langlois C.Synthesis and processing of metallic nano-powders for the study of their mechanical and magnetic properties[J].Materials Science Forum,2003,426/432(3):2411-2416.
【30】Hashimoto,Noritsugu,Hashimoto.Preparation of silver thin films consisting of nano-sized particles by the evaporation-condensation method and its linear and nonlinear optical properties[J].Journal of the Ceramic Society of Japan,2004,112:204-209.
【2】徐存英,王真,洪品杰.纳米粉体材料的制备[J].云南民族学院学报,1998,7(1):65-66.
【3】Takaki S,Yatsuya S.Nanoparticle produced by sputtering[C]//14th International Congress on Electron Microscopy.Cancun,Mexico:[s.n] 1998:469-470.
【4】杜芳林,崔作林,张志锟,等.纳米铜的制备、结构及催化性能[J].分子催化,1997,18(3):46-48.
【5】魏胜,王朝阳,黄勇,等.蒸发冷凝法制备纳米Al粉及其热反应特性研究[J].原子能科学技术,2002,36(4):367-370.
【6】胡军辉,吴润,黄为,等.激光感应复合加热蒸发冷凝法制备超微锌粉[J].激光技术,2000,24(2):100-101.
【7】魏智强,马军,冯旺军,等.等离子体制备银纳米粉末的研究[J].贵金属,2004,25(3):29-32.
【8】鲍久圣,刘同冈,杨志伊,等.蒸发冷凝法制备纳米粉体实验装置的研制[J].机电产品开发与创新,2004,17(5):18-19.
【9】刘同冈,鲍久圣,杨志伊.直流钨电弧法制备碳包覆铁纳米微粒的研究[J].中国矿业大学学报,2007,36(2):201-204.
【10】Yatsuya S.Growth of fullerene nanoparticles prepared by the gas-evaporation technique[J].Journal of Materials Science,1998,33(24):5843-5847.
【11】任瑞铭.纳米粉体材料制备技术[J].大连铁道学院学报,1999,20(3):69-72.
【12】陆必志,陈振兴,黄巧萍,等.纳米片状铝粉的制备及其发展动态[J].粉末冶金工业,2004,14(2):41-44.
【13】黄开金,谢长生,许德胜.激光蒸发冷凝法制备纳米颗粒的研究现状[J].激光技术,2004,28(1):5-11.
【14】陆必志,陈振兴.蒸发-冷凝法制备超细鳞片状锌粉[J].粉末冶金工业,2005,15(2):5-8.
【15】Champion,Yannick.Evaporation and condensation for metallic nanopowders[J].Annales de Chimie:Science des Materiaux,2006,31(3):281-29.
【16】Yan Hongge,Li Yunong,Chen Qing.Powder preparation with evaporation and condensation method[J].Journal of Hunan University Natural Sciences,2005,32(2):85-89.
【17】钟胜,戴永年.真空蒸发冷凝制备超细锌粉的研究[J].昆明理工大学学报,1998,23(3):48-52.
【18】陈允鸿,姜玉梅,朱骏,等.FeNi合金超细微粒的蒸发冷凝法制备及其微结构[J].南京大学学报,1994,30(4):600-605.
【19】陈允鸿,姜玉梅.蒸发冷凝法中气体压强和蒸发温度对粒子大小的影响[J].功能材料,1994,25(5):418-420.
【20】曹立宏,傅磊,樊友三.直流电弧等离子体制备TiN纳米粉末的研究[J].硅酸盐学报,1997,25(1):106-109.
【21】Singh,Yogendra.Approaches to increasing yield in evaporation/condensation nanoparticle generation[J].Journal of Aerosol Science,2002,33(9):1309-1325.
【22】鲍久圣,刘同冈,杨志伊,等.蒸发冷凝法制备纳米粉体反应容器中的温度场研究[J].机械科学与技术,2006,25(11):1334-1337.
【23】Yokoyama,Saito,Katsuyoshi.Evaporation rate of molten iron in Ar+O2 gas stream and characteristics of condensed particles[J].Journal of the Japan Institute of Metals,1995,59(10):1030-1035.
【24】陈允鸿,陈庆琉,邓桂昌,等.Fe-29wt%Ni合金超细微粒的压力效应[J].应用科学学报,1996,14(4):427-430.
【25】陈允鸿,朱骏,王锦辉,等.Fe-47wt%Ni纳米晶粉芯磁谱及其压力效应[J].功能材料,1997,28(6):655-657.
【26】夏辉,谢长生,胡军辉.表面钝化处理对纳米Zn粉抗氧化性能的影响[J].金属热处理学报,2000,21(3):17-20.
【27】苏眆,谢斌,陈允鸿.坡莫合金纳米粉的恒导磁性及其磁导率的压力、频率特性[J].高压物理学报,1995,9(4):247-255.
【28】朱骏,陈允鸿,王锦辉,等.退火对Fe-47%wtNi合金超细微粒压结体高频特性的影响[J].功能材料,1997,28(4):441-443.
【29】Champion Y,Bonnentien J-L,Langlois C.Synthesis and processing of metallic nano-powders for the study of their mechanical and magnetic properties[J].Materials Science Forum,2003,426/432(3):2411-2416.
【30】Hashimoto,Noritsugu,Hashimoto.Preparation of silver thin films consisting of nano-sized particles by the evaporation-condensation method and its linear and nonlinear optical properties[J].Journal of the Ceramic Society of Japan,2004,112:204-209.
相关信息
