Effect of Temperature on Creep Rate of Three-Dimensional C/SiC Composites
摘 要
采用高温真空蠕变试验机研究了1 300℃和1 500℃下三维(3D)C/SiC复合材料的蠕变行为,分析了温度对该复合材料蠕变速率的影响,并通过扫描电镜和透射电镜分析了蠕变前后复合材料的显微结构.结果表明:不同温度下该复合材料的高温蠕变曲线均由减速蠕变阶段和稳态蠕变阶段两部分组成,试样断裂前没有出现加速蠕变阶段;温度越高,靠近SiC基体处的热解碳界面相由乱层石墨组织转变为高度取向排列的石墨片层组织的厚度就越大,从而导致复合材料界面滑移阻力更低,蠕变速率更快.
Abstract
The creep behavior of three-dimensional(3D)C/SiC composites was examined at 1 300℃ and 1 500℃ using vacuum high-temperature creep testing machine.The effect of temperature on the creep rate of the composites was also investigated.Microstructure of the composites before and after creep testing was analyzed by means of SEM and TEM.The results indicate that the creep curves of 3D C/SiC composites were composed of two stages including deceleration creep stage and steady state creep stage,and no accelerated creep stage was observed until the fracture of the specimens.With the increase of temperature,the interfacial sliding resistance decreased due to the increase of the thickness of highly oriented lamellar graphite transformed from turbostratic graphite in the pyrolytic carbon interphase near the SiC matrix,resulting in a more rapid creep rate of 3D C/SiC composites.
中图分类号 TB332
所属栏目 试验研究
基金项目 国家自然科学基金资助项目(90716023);西安石油大学科技基金研究项目(Z08102)
收稿日期 2009/6/20
修改稿日期 2010/2/5
网络出版日期
作者单位点击查看
备注张钧(1976-),男,陕西咸阳人,讲师,博士.
引用该论文: ZHANG Jun,QIAO Sheng-ru,ZHANG Li-tong. Effect of Temperature on Creep Rate of Three-Dimensional C/SiC Composites[J]. Materials for mechancial engineering, 2010, 34(7): 16~19
张钧,乔生儒,张立同. 温度对三维C/SiC复合材料蠕变速率的影响[J]. 机械工程材料, 2010, 34(7): 16~19
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参考文献
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【3】ABBE F,CARIN R,CHERMANT J L.Tensile and compre-ssive creep characteristics from bending tests,application to SiC-SiC composites[J].J Eur Ceram Soc,1989,5(3):201-205.
【4】ABBE F,VICENS J,CHERMANT J L.Creep behaviour and microstructural characterization of a ceramic matrix composite[J].J Mater Sci Lett,1989,8(9):1026-1028.
【5】HOLMES J.Technique for tensile fatigue and creep testing of fiber-reinforced ceramics[J].J Compos Mater,1992,26(6):916-933.
【6】WU X,HOLMES J.Tensile creep and creep-strain recovery behavior of silicon carbide fiber/calcium aluminosilicate matrix ceramic composites[J].J Am Ceram Soc,1993,76(10):2695-2700.
【7】BOITIER G,CHERMANT J L,VICENS J.Understanding the creep behavior of a 2.5D Cf/SiC composite.II.experimental specifications and macroscopic mechanical creep responses[J].Mat Sci Eng A,2000,289(1):265-275.
【8】BOITIER G,VICENS J,CHERMANT J L.Understanding the creep behavior of a 2.5 D Cf/SiC composite.III.from mesoscale to nanoscale microstructural and morphological investigation towards creep mechanism[J].Mat Sci Eng A,2001,313(1/2):53-63.
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【10】BOITIER G,VICENS J,CHERMANT J L.Nanocreep of carbon fibers in 2.5D Cf/SiC[J].Key Eng Mater,1999,164/165:337-340.
【11】BOITIER G,VICENS J,CHERMANT J L.Nanostructure study by TEM and HREM of carbon fibres in Cf/SiC compo-sites[J].J Mater Sci Lett,1997,16(16):1402-1405.
【12】CHERMANT J L.Creep behaviour of ceramic matrix composites[J].Silic Indus,1995,60(9/10):261-273.
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