压痕硬度测试法的主要研究内容及其应用
APPLICATION AND STUDYING CURRENT STATUS OF THE INDENTATION HARDNESS TESTING
摘 要
详细分析了压痕硬度测试方法自发展以来所研究的主要内容,即建立不同硬度之间的关系、硬度与弹性性能的关系、硬度与强度的关系、硬度与蠕变性能的关系、材料显微组织对硬度的影响以及硬度在薄膜力学测试中的应用等。其中,研究重点主要集中在建立硬度与力学性能参量之间的数学关系方面,即通过压痕硬度测试中获取的有关数据来得到相关的力学参量。同时提出了压痕硬度测试法的研究现状及存在的主要问题。
纳米压痕硬度
力学性能
薄膜力学
硬度测试
Indentation hardness
nano-indentation hardness
mechanics performances
film mechanics
hardness testing
Abstract
The indentation experiment plays a very important role in mechanical performance testing. In recent years,various forms of indentation testing have been increasingly used to determine the material properties of specimens. The review surveys the application and significance of the techniques since developing indentation testing method,particularly the nano-indentation method. Although a lot of work study was researched,such as studying on the relation between one hardness value and the other one,the effect of the material microcosmic structure to hardness value,the application of hardness to test thin film mechanical properties,and so on,the technique was mainly used to deduce the elastic,plastic,fracture,creep,and adhesive properties of a great variety of materials,ranging from metals,ceramics,polymers,to biomaterials. Meanwhile,the study current status and the problem were discussed in instrumented indentation experiments. The technique has been extended to the testing of coating systems in order to calculate the individual properties of the thin coatings and the substrates.
中图分类号 TB302.3
所属栏目 综述
基金项目 天津市自然科学重点基金(08JCZDJC 16100)
收稿日期 2007/9/14
修改稿日期
网络出版日期
作者单位点击查看
备注刘美华(1963-),女,副教授,博士。
引用该论文: LIU Mei-hua,LI Hong-qi,JI Hong-wei,TONG Jing-wei. APPLICATION AND STUDYING CURRENT STATUS OF THE INDENTATION HARDNESS TESTING[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2008, 44(9): 485～490
刘美华,李鸿琦,计宏伟,佟景伟. 压痕硬度测试法的主要研究内容及其应用[J]. 理化检验－物理分册, 2008, 44(9): 485～490
被引情况:
【1】许好好,金杰,叶笃毅, "深度-敏感压痕测试技术在高温炉管力学性能变化研究中的应用",理化检验－物理分册 51, 684-687(2015)
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参考文献
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【25】李河清,蔡 珣,陈秋龙. 纳米压入技术表征薄膜(涂层)的力学性能[J]. 材料热处理学报,2001,22(4): 52-55．
【26】李河清,蔡 珣,马 峰,等.影响薄膜(涂层)硬度测试的因素[J]. 材料保护,2001,34(9):47-49．
【27】Brotzen F R. Mechanics testing of thin films[J]. International Material Reviews,1994,39(1): 24-44．
【28】陈隆庆,赵明嗥,张统一. 薄膜的力学测试技术[J]. 机械强度,2001,23(4): 413-429．
【29】Joslin D L,Oliver W C.A new method for analyzing data from continuous depth -sensing micro-indentation tests[J]. J Mater Res,1990,5(1):123-126．
【30】Pharr G M,Oliver W C. On the generality of the relationship among stiffness contact area and elastic modulus during indentation[J]. J Mater Res,1992,7(3): 613-617．
【31】Chen Y T. Cheng C M. Relationships between hardness,elastic modulus,and the work of indentation[J]. Appl Phys Lett,1998,73(5):614-616 ．
【2】杨 迪. 金属硬度实验[M]. 北京: 中国计量出版社,1983．
【3】Bhushan B,Gupta B K. Handbook of Tribology [M]. New York: McGraw-Hill,1991．
【4】虞伟良. 硬度测试技术的新动态与发展趋势[J]. 理化检验-物理分册,2003,39(8): 401-406．
【5】韩德伟. 金属的硬度及其试验方法[M]. 长沙: 湖南科学技术出版社,1983．
【6】杨 迪,李福欣. 显微硬度试验[M]. 北京: 中国计量出版社,1988: 1．
【7】完卫国. HS与HRC,HV硬度互换的数学公式[J]. 理化检验-物理分册,1993,29(6): 53．
【8】苑凤忠. 球形压头布氏硬度与洛氏硬度值之间的理论关系[J]. 山东工业大学学报,1989,19(3): 69-74．
【9】郑远谋. 抛光时间和表面粗糙度对铸铁材料硬度测试数据的影响[J]. 机械强度,1992,11(2): 63-68．
【10】林丽华,陈立功,顾明元. 静载压痕残余应力测量的简化模型[J]. 上海交通大学学报,1998,32(2):91-94．
【11】Tabor D. The hardness of metals[M]. Oxford: Clarendon Press,1952．
【12】Oliver W C,Pharr G M. An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments [J]. J Mater Res,1992,7(6): 1564-1583．
【13】Chang Y T,Chang C M. Relationship between hardness,elastic modulus and the work of indentation[J]. Appl Phys Lett,1998,73: 614-616．
【14】王长春.LD合金抗拉强度与硬度关系探讨[J]. 理化检验-物理分册,1996,32(6): 50．
【15】顾丽英. GT60-2抗拉强度与硬度关系的探讨[J]. 理化检验-物理分册,1995,31(5): 46．
【16】Juhasz A,Tasnadi P. Investigation of the superplasticity of tin-lead eutectie by impression creep tests[J]. J Mater Sci,1986,21(10): 3287-3291．
【17】Yang F Q,Li J C M. Computer of impression creep using the hyperbolie sine stress law[J]. Mater Sci Eng,1995,A201: 50-57．
【18】Raman V,Berriche R. An investigation of the creep processes in tin and aluminum using a depth-sensing indentation technique[J]. J Mater Res,1992,7(3): 627-638．
【19】万建松,岳珠峰.采用压痕实验获得材料性能的研究现状[J]. 实验力学,2002,17(2): 131-139．
【20】Chudoba T,Richter F. Investigation of creep behaviour under load during indentation experiments and its influence on hardness and modulus results[J]. Surface and Coatings Technology,2001,148(2,3):191．
【21】Li J C M. Impression creep and other localized tests[J]. Materials Science and Engineering A,2002,322(1,2): 23-42 ．
【22】刘 澄,张国定. 用超显微硬度方法研究复合材料微区力学性能[J]. 机械工程学报,1999,23(2): 20-23．
【23】张福勤,李怀明,杨 让. 钢轨的疲劳寿命、磨损抗力与组织和硬度的关系[J]. 钢铁,1991,26(7): 43-47．
【24】田永生. 铸铁硬度与切削加工性能的关系[J].钢铁研究学报,1998,10(2): 74-76．
【25】李河清,蔡 珣,陈秋龙. 纳米压入技术表征薄膜(涂层)的力学性能[J]. 材料热处理学报,2001,22(4): 52-55．
【26】李河清,蔡 珣,马 峰,等.影响薄膜(涂层)硬度测试的因素[J]. 材料保护,2001,34(9):47-49．
【27】Brotzen F R. Mechanics testing of thin films[J]. International Material Reviews,1994,39(1): 24-44．
【28】陈隆庆,赵明嗥,张统一. 薄膜的力学测试技术[J]. 机械强度,2001,23(4): 413-429．
【29】Joslin D L,Oliver W C.A new method for analyzing data from continuous depth -sensing micro-indentation tests[J]. J Mater Res,1990,5(1):123-126．
【30】Pharr G M,Oliver W C. On the generality of the relationship among stiffness contact area and elastic modulus during indentation[J]. J Mater Res,1992,7(3): 613-617．
【31】Chen Y T. Cheng C M. Relationships between hardness,elastic modulus,and the work of indentation[J]. Appl Phys Lett,1998,73(5):614-616 ．
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