千山野菊花挥发性化学成分的提取与分析
EXTRACTION AND ANALYSIS OF VOLATILE CONSTITUENTS IN THE CHRYSANTHEMUM INDICUM L.FROM QIANSHAN
摘 要
报道了用蒸馏-萃取法和同时蒸馏-萃取法提取千山野菊花中挥发性物质,测得用两种方法提取的千山野菊花挥发油含量分别为6.1 % 和7.0%,用GC/MS法从千山野菊花挥发油中分别分离并确定出34种和29种化学成分,分别占千山野菊花挥发油总检出量的89.47%和90.72%,用峰面积归一化法得出各类化学成分在挥发油中的相对百分含量.
挥发性物质
同时蒸馏-萃取法
气相色谱-质谱
Chrysanthemum indicum L.
Volatile constituent
Distillation combined with extraction
GC/MS
Abstract
A method of steam distillation followed by solvent extraction and a combined method of distillation with solvent extraction were separately adopted for the collection of volatile constituents in Chrysanthemum indicum L.from Qianshan.The yields of the oily collection were 6.1% for the former method and 7.0% for the combined method respectively.GC/MS was used for the identification of the chemical constituents in the volatile oil and a method of normalized peak area was used for the determination of the percentage content.Thirty-four constituents with content of 89.47% in the oil collected by the former method and 29 constituents with content of 90.72% in the oil collected by the later method were identified.
中图分类号 Q657.63
所属栏目 工作简报
基金项目 辽宁省教育厅科学技术基金资助课题(20331079)
收稿日期 2004/11/22
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备注回瑞华(1945-),女,回族,辽宁海城市人,教授,从事有机分析及天然产物化学教学与研究.
引用该论文: HUI Rui-hua,HOU Dong-yan,LI Tie-chun,ZHU Yong-qiang,LIU Xiao-yuan. EXTRACTION AND ANALYSIS OF VOLATILE CONSTITUENTS IN THE CHRYSANTHEMUM INDICUM L.FROM QIANSHAN[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2006, 42(8): 640～643
回瑞华,侯冬岩,李铁纯,朱永强,刘晓媛. 千山野菊花挥发性化学成分的提取与分析[J]. 理化检验－化学分册, 2006, 42(8): 640～643
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参考文献
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【3】回瑞华,侯冬岩,李铁纯.苦杏仁挥发油化学成分的微波-同时蒸馏萃取GC-MS分析[J].分析测试学报,2003,22(1):55-57.
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【5】回瑞华,侯冬岩,李铁纯,等.肉苁蓉挥发性化学成分分析[J].分析化学,2003,31(5):601-603.
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【7】江苏新医学院.中药大辞典(附编)[M].上海:上海科学技术出版社,1979:395-587.
【8】施钧慧,汪聪慧.香料质谱图集[Z].北京:中国质谱学会,1992:39.
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