Application of Fourier Transform-Near Infrared Spectrometry to Qualitative Analysis of Pilose Antler
摘 要
利用近红外光谱(NIRS)和OPUS/Ident软件,通过计算采集到的样品的近红外光谱图之间的欧氏距离来反映不同鹿茸样品间的差异,对不同产地、不同种类的鹿茸进行了分类鉴别(Identification).结果表明,与传统方法繁琐复杂,主观性大相比,近红外光谱法能实现鹿茸的快速、无损和可靠的分析鉴别,为鹿茸的质量鉴别提供了一个客观有效的方法.
Abstract
In the qualitative analysis of pilose antler by fourier transform-near infrared spectrometry (FT-NIRS) with the software OPUS/Ident,discrimination and identification of samples of different species and geographical origins was performed by collecting their NIR spectra and calculating the Euclidean distances,i.e the spectral distances D,among the spectra. It was proved by the analytical results that the FT-NIRS is a better and more reliable method,for its special features of rapidity and non-destructive,in comparing with the conventional methods,which are laborious and time-consuming. It was also shown that the results obtained by FT-NIRS were more objective than those obtained by the conventional methods,which depend much on the subjective judgement of experienced analytical chemists.
中图分类号 O657.33
所属栏目 工作简报
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收稿日期 2005/9/17
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备注毛建江(1979-),男,江西人,硕士研究生,主要从事分子光谱分析结合化学计量学的研究与应用.
引用该论文: MAO Jian-jiang,ZHANG Yu-jie,XU Jing-wei. Application of Fourier Transform-Near Infrared Spectrometry to Qualitative Analysis of Pilose Antler[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2007, 43(1): 33~36
毛建江,张玉杰,徐经伟. 傅立叶近红外光谱法用于鹿茸的定性分析[J]. 理化检验-化学分册, 2007, 43(1): 33~36
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参考文献
【1】陆婉珍,袁洪福,徐广通,等.现代近红外光谱分析技术[M].北京:中国石化出版社,2000.
【2】Cho Changhee,Woo Youngah,Kim Hyojin,et al. Rapid qualitative and quantitative evaluation of deer antler (Cer-us elaphus) using near-infrared reflectance spectroscopy[J]. Microchemical Journal,2001,68:189.
【3】杨南林,程翼宇,吴永江.中药材三七中皂苷类成分的近红外光谱快速无损分析新方法[J].化学学报,2003,61(3):393.
【4】Woo Youngah,Kim Hyojin,Cho Junghwan,et al. Discrimination of herbal medicines according to geographical origin with near infrared reflectance spectroscopy and pattern recognition techniques[J]. Journal of Pharmaceutical and Biomedical Analysis,1999,21:407-413.
【5】Woo Youngah,Kim Hyojin,Cho Junghwan. Identification of herbal medicines using pattern recognition techniques with near-infrared reflectance spectra[J]. Microchemical Journal,1999,63:61.
【6】沈保安,刘晓龙,吴秀清,等.中药鉴定现代研究[M].北京:中国中医药出版社,1998.
【7】宏惠田,李桂兰.鹿茸片及其伪品的鉴定[J].天津药学,1994,6(4):32.
【8】郑俊民,张连珠,周 晖.用热分析技术和红外光谱法鉴别花鹿茸的研究[J].沈阳药科大学学报,13(3):196.
【9】苗明三,李振国.现代实用中药质量控制技术[M].北京:人民卫生出版社,2000.
【10】Howard L Mark,Divid Tunnell. Qualitative near-infrared reflectance analysis using mahalanobis distance[J]. Analytical Chemistry,1985,57:1449.
【11】Ian A Cowe,James W Mcnicol. The use of principal components in the analysis of near-infrared spectra[J]. Applied Spectroscopy,1985,39(2):257.
【12】钟蕾,朱斌,宓鹤鸣,等.近红外漫反射光谱聚类分析用于血竭的鉴别[J].理化检验-化学分册,2004,40(1):9.
【13】潘忠孝,司圣柱,聂圣哲,等.化学因子分析[M].合肥:中国科学技术大学出版社,1992.
【2】Cho Changhee,Woo Youngah,Kim Hyojin,et al. Rapid qualitative and quantitative evaluation of deer antler (Cer-us elaphus) using near-infrared reflectance spectroscopy[J]. Microchemical Journal,2001,68:189.
【3】杨南林,程翼宇,吴永江.中药材三七中皂苷类成分的近红外光谱快速无损分析新方法[J].化学学报,2003,61(3):393.
【4】Woo Youngah,Kim Hyojin,Cho Junghwan,et al. Discrimination of herbal medicines according to geographical origin with near infrared reflectance spectroscopy and pattern recognition techniques[J]. Journal of Pharmaceutical and Biomedical Analysis,1999,21:407-413.
【5】Woo Youngah,Kim Hyojin,Cho Junghwan. Identification of herbal medicines using pattern recognition techniques with near-infrared reflectance spectra[J]. Microchemical Journal,1999,63:61.
【6】沈保安,刘晓龙,吴秀清,等.中药鉴定现代研究[M].北京:中国中医药出版社,1998.
【7】宏惠田,李桂兰.鹿茸片及其伪品的鉴定[J].天津药学,1994,6(4):32.
【8】郑俊民,张连珠,周 晖.用热分析技术和红外光谱法鉴别花鹿茸的研究[J].沈阳药科大学学报,13(3):196.
【9】苗明三,李振国.现代实用中药质量控制技术[M].北京:人民卫生出版社,2000.
【10】Howard L Mark,Divid Tunnell. Qualitative near-infrared reflectance analysis using mahalanobis distance[J]. Analytical Chemistry,1985,57:1449.
【11】Ian A Cowe,James W Mcnicol. The use of principal components in the analysis of near-infrared spectra[J]. Applied Spectroscopy,1985,39(2):257.
【12】钟蕾,朱斌,宓鹤鸣,等.近红外漫反射光谱聚类分析用于血竭的鉴别[J].理化检验-化学分册,2004,40(1):9.
【13】潘忠孝,司圣柱,聂圣哲,等.化学因子分析[M].合肥:中国科学技术大学出版社,1992.
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