ICP-AES Determination of 7 Foreign Elements in Barium Titanate Nano-powder
摘 要
钛酸钡纳米粉体样品用盐酸溶解,在所得样品溶液中用电感耦合等离子体原子发射光谱法测定了以氧化物存在于样品中的7种杂质元素(包括镁、锶、钾、钠、铝、硅及铁),对测定的光谱条件进行了试验并优化达到上述各元素的测定上限为0.1%(质量分数).测得方法的检出限(3S/b)为(单位μg·L-1):2.0(铝),1.0(铁),20.0(钾),0.2(镁),4.0(钠),3.0(硅)及0.5(锶).应用此方法分析了两件实样,所得结果的相对标准偏差(n=6)小于等于2.0%,对其中4种杂质元素(镁、钾、钠和锶)同时用HG/T 3587-1999标准中的方法作分析校核,所得结果与此方法结果一致.
Abstract
Sample of the nano-powdery barium titanate was dissolved in hydrochloric acid and the solution obtained was used for determination of 7 foreign elements (including Mg,Sr,K,Na,Al,Si and Fe) present as their oxides in the sample by ICP-AES.Spectrometric conditions for the determination were tested and optimized to have the upper limit of determination set at 0.1% (mass percentage).Detection limits (3S/b) were found to be (in μg·L-1) 2.0(Al),1.0(Fe),20.0(K),0.2(Mg),4.0(Na),3.0(Si) and 0.5(Sr).Two samples of the barium titanate analyzed for contents of the 7 elements (as oxides),giving values of RSD′s (n=6) ≤2.0%.Four of the 7 elements,i.e.Mg,K,Na and Sr,were determined by the present method and also by the standard methods given in HG/T 3587-1999 in parallel,consistent results were obtained.
中图分类号 O657.31
所属栏目 工作简报
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收稿日期 2006/12/26
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备注董发昕(1958-),男,西安市人,高级工程师,主要从事原子光谱分析.
引用该论文: DONG Fa-xin,HU Huai-ming,JA Ying-qi. ICP-AES Determination of 7 Foreign Elements in Barium Titanate Nano-powder[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2008, 44(8): 773~774
董发昕,胡怀明,贾婴奇. 电感耦合等离子体原子发射光谱法测定钛酸钡纳米粉体中7种杂质元素[J]. 理化检验-化学分册, 2008, 44(8): 773~774
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参考文献
【1】HG/T 3587-1999电子工业用高纯钛酸钡[S].
【2】GB/T 3049-1986化工产品中铁含量测定的通用方法[S].
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【5】魏春艳,董玉兰,刘刚耀.ICP-AES法测定铁矿石中SiO2,CaO,MgO,Al2O3,MnO和TiO2[J].冶金分析,2004,24(1):58-60.
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【2】GB/T 3049-1986化工产品中铁含量测定的通用方法[S].
【3】戴亚明,陶美娟,马冲光.电感耦合等离子体发射光谱法测定镁合金中铝锌锰硅铜镍铍锆[J].理化检验-化学分册,2004,40(3):155-157.
【4】何海成,黄志荣,黄新平,等.电感耦合等离子体发射光谱法测定硅铝铁合金中的多种元素[J].分析科学学报,2004,20(2):142-144.
【5】魏春艳,董玉兰,刘刚耀.ICP-AES法测定铁矿石中SiO2,CaO,MgO,Al2O3,MnO和TiO2[J].冶金分析,2004,24(1):58-60.
【6】沈良华,赵占良,徐子培.IRIS电感耦合等离子体原子发射光谱培训教程[Z].美国热电(中国)公司,2002:38.
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