AAS Determination of Eight Trace Elements in Hawthorn with Microwave Assisted Sample Digestion
摘 要
采用微波消解法处理山楂样品,通过火焰原子吸收光谱法测定山楂中镁、钙、铁、锌、锰、铅、铬和铜8种金属元素的含量.对硝酸与高氯酸的体积比、消解功率和消解时间进行了试验并予以优化.吸光度与8种金属元素的质量浓度在一定范围内呈线性关系.应用此法测得山楂中只含有镁、钙、铁、锌和锰5种元素,测得结果分别为1.49,3.15,0.86,0.003,0.052 mg·g-1,加标回收率在94.2%~109.3%之间.
Abstract
Trace amounts of Mg,Ca,Fe,Zn,Mn,Pb,Cr and Cu in hawthorn were determined by flame atomic absorption spetrometry. The sample was treated by microwave assisted sample digestion. Influential factors,including the volume ratio of HNO3 and HClO4 used for sample digestion,power of microwave in digestion,and time of digestion were studied and optimized. Linear relationships between values of absorbances and mass concentrations of the 8 metal elements were obtained in a definite range. Only 5 elements,i.e.,Mg,Ca,Fe,Zn and Mn,were found in hawthorn as determined by the proposed method,and their contents obtained were 1.49,3.15,0.86,0.003 2 and 0.052 mg·g-1 respectively. Values of recovery found by standard addition method were in the range of 94.2%-109.3%.
中图分类号 O657.31
所属栏目 工作简报
基金项目 山西省高校科技研究开发项目(No20051260)
收稿日期 2008/4/7
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备注李满秀(1955-),男,山西省原平市人,教授,研究方向为光谱分析.
引用该论文: LI Man-xiu,XIN Sheng. AAS Determination of Eight Trace Elements in Hawthorn with Microwave Assisted Sample Digestion[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2009, 45(7): 820~821
李满秀,辛胜. 微波消解-火焰原子吸收光谱法测定山楂中八种微量元素的含量[J]. 理化检验-化学分册, 2009, 45(7): 820~821
被引情况:
【1】刘树彬,郧海丽,冯俊霞,于宏伟, "原子吸收光谱法在测定食品中金属元素的研究进展",理化检验-化学分册 46, 850-854(2010)
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