一种抛光蜡的化学组分分析
Analysis for Components of a Polishing Wax
摘 要
采用分级溶剂抽提技术为分离方法,以傅里叶变换红外光谱法为主要分析手段,结合气相色谱、气相色谱-质谱、X-射线衍射光谱以及等离子体发射光谱等,对一种进口工业抛光蜡进行了组成剖析,最终得到6种主要组成:棕榈酸和硬脂酸、氢化动物油、松香树脂、石蜡、α-型二氧化硅和以三氧化二铁为主的无机金属氧化物.
组分分析
抛光蜡
FTIR
Componental analysis
Polishing wax
Abstract
Componental analysis of an imported industrial polishing wax was performed by using Fourier transform IR (FTIR) spectrometry as main analytical method and using GC-MS,XRD and ICP-AES as supplementary methods.Six main components,i.e.,palmitic acid,stearic acid,hydrogenated tallow oil,galipot resin,wax and α-silicon dioxide,were found,and in addition ferric oxide (Fe2O3) was found as a main inorganic metal oxide.Various components in the sample were separated by classification solvent extraction technique before the identification analysis.
中图分类号 O657.33
所属栏目 工作简报
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收稿日期 2008/3/19
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备注马慧莲(1979-),女,回族,辽宁大连人,助理研究员,硕士,主要从事应用光谱与色谱分析研究.
引用该论文: MA Hui-lian,TIAN Yu-zeng,HUANG Wei-dong,CHEN Ji-ping. Analysis for Components of a Polishing Wax[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2009, 45(8): 965～967
马慧莲,田玉增,黄威东,陈吉平. 一种抛光蜡的化学组分分析[J]. 理化检验－化学分册, 2009, 45(8): 965～967
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参考文献
【1】曾燕,陈志祥,刘宏江,等.不锈钢用抛光蜡的研制[J].广东有色金属学报,2006,16(1):16-18．
【2】HANSEN D L.Sprouse collection of infrared spectra,Book Ш: surface active agents (DB)[M].Paoli USA: Sprouse Scientific Systems,Inc,1988:362．
【3】HUMMEL D O.Atlas of polymer and plastics anaylsis (DB)[M].Volume 2,Weinheim Germany: Verlag Chemic GmbH,1984:2548．
【4】SCHOLL E K.Infrared analysis of polymers,resins and additives an atlas (DB)[M].Volume 2,Munich Germany: Carl Hanser Verlag,1973:2315．
【5】黄志超,许栋强.精细化工应用配方3000例[M].广东:广东科技出版社,1990:420-423．
【2】HANSEN D L.Sprouse collection of infrared spectra,Book Ш: surface active agents (DB)[M].Paoli USA: Sprouse Scientific Systems,Inc,1988:362．
【3】HUMMEL D O.Atlas of polymer and plastics anaylsis (DB)[M].Volume 2,Weinheim Germany: Verlag Chemic GmbH,1984:2548．
【4】SCHOLL E K.Infrared analysis of polymers,resins and additives an atlas (DB)[M].Volume 2,Munich Germany: Carl Hanser Verlag,1973:2315．
【5】黄志超,许栋强.精细化工应用配方3000例[M].广东:广东科技出版社,1990:420-423．
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