Preparation and Properties of 6.5%Si Electrical Steel Composite Plate
摘 要
以普通硅钢和硅铁合金为原料,采用包覆浇铸法制备具有三层结构的高硅电工钢铸坯,之后结合传统的轧制工艺和扩散退火工艺获得了6.5% Si电工钢复合板,利用光学显微镜和扫描电镜研究了其显微组织和硅元素的分布,并对其磁性能进行了测试。结果表明:采用上述工艺方法成功制备出了0.5 mm厚的电工钢复合板;经1 200℃×75 min扩散退火后,电工钢复合板中的硅元素发生了完全扩散,复合板由三层结构变成单层结构,整体硅元素质量分数约为6.5%;6.5% Si电工钢复合板的铁损P1.5/50为2.68~2.72 W·kg-1,磁感应强度B8为1.370~1.378 T、B50为1.610~1.625 T;与0.34 mm厚的Fe-6.5% Si合金相比,复合技术制备的6.5% Si电工钢复合板的磁感应强度较高,但铁损也略高。
Abstract
High silicon electrical steel ingot with three-layer structure was prepared by clad casting using common silicon steel and silicon ferrosilicon alloy, then 6.5%Si electrical steel composite plate was obtained by traditional rolling process and diffusion annealing process. Microstructure and Si element distribution were studied by optical microscope and scanning electrical microscope. Magnetic properties were also tested. The results show that electrical steel composite plate with 0.5 mm thickness could be prepared by this method successfully. After 1 200℃×75 min diffusion annealing treatment, Si element diffused completely and three layers of composite plate was changed into single layer gradually, while the content of Si element was about 6.5wt.%. The value of iron loss P1.5/50 was 2.68-2.72 W·kg-1 and the values of magnetic induction B8 was 1.370-1.378 T, B50 was 1.610-1.625 T for 6.5%Si electrical steel composite plate. Compared with Fe-6.5%Si alloy whose thickness was 0.34 mm, 6.5%Si electrical steel composite plate prepared by this method had a higher magnetic induction but greater iron loss.
中图分类号 TM275 DOI 10.11973/jxgccl201707010
所属栏目 新材料 新工艺
基金项目 西安石油大学《材料科学与工程》省级优势学科资助项目;西安石油大学青年科技创新基金资助项目(2016BS21)
收稿日期 2016/5/11
修改稿日期 2017/6/6
网络出版日期
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备注姬帅(1985-),男,山东菏泽人,讲师,博士
引用该论文: JI Shuai. Preparation and Properties of 6.5%Si Electrical Steel Composite Plate[J]. Materials for mechancial engineering, 2017, 41(7): 49~53
姬帅. 6.5% Si电工钢复合板的制备与性能[J]. 机械工程材料, 2017, 41(7): 49~53
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参考文献
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【2】YUAN W J, LI J G, SHEN Q, et al. A study on magnetic properties of high Si steel obtained through powder rolling processing[J]. Journal of Magnetism and Magnetic Materials, 2008, 320(1):76-80.
【3】YE F, LIANG Y F, WANG Y L, et al. Fe-6.5wt.%Si high silicon steel sheets produced by cold rolling[J]. Materials Science Forum, 2010, 638/639/640/641/642:1428-1433.
【4】ZHANG Z, WANG W, FU H, et al. Effect of quench cooling rate on residual stress, microstructure and mechanical property of an Fe-6.5Si alloy[J]. Materials Science and Engineering A, 2011, 530(11):519-524.
【5】SHIN J S, BAE J S, KIM H J, et al. Ordering-disordering phenomena and micro-hardness characteristics of B2 phase in Fe-(5-6.5%)Si alloys[J]. Materials Science and Engineering A, 2005, 407(1/2):282-290.
【6】ROS T, RUIZ D, HOUBAERT Y, et al. Study of ordering phenomena in high silicon electrical steel (up to 12.5at%) by m ssbauer spectroscopy[J]. Journal of Magnetism and Magnetic Materials, 2002, 242/243/244/245:208-211.
【7】JI S, HAN J T, LIU J, et al. Effect of diffusion annealing on defects reduction of 6.5wt% high silicon steel composite plate after hot deformation[J]. Advanced Materials Research, 2014, 941/942/943/944:338-342.
【8】JI S, HAN J T, LIU J. Fabrication of 6.5wt%Si composite plate by coat casting and hot deformation processes[J]. Advanced Materials Research, 2014, 902:7-11.
【9】JI S, HAN J T, LIU J, et al. Iron loss measurement on 6.5wt%Si composite plate prepared by clad casting and conventional rolling processes[J]. Advanced Materials Research, 2014,941/942/943/944:348-353.
【10】JI S, HAN J T, LIU J, et al. Production of 6.5wt%Si composite thin sheet by cold rolling process[J]. Advanced Materials Research, 2014, 941/942/943/944:354-359.
【11】高超, 苏芳臣, 相颖杰, 等. 不同冷轧退火工艺下薄带连铸无取向硅钢的组织和磁性能[J]. 机械工程材料, 2015,39(12):12-16.
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