Comparison between Dumas Combustion Method and Continuous Flow Method for Determination of Total Nitrogen in Reconstituted Tobacco
摘 要
为提高检测再造烟叶中总氮含量的检测效率,对杜马斯燃烧法(简称D法)和连续流动法(简称L法)进行了对比研究,并初步探索了转换D法结果来代替L法结果的方法。结果表明:杜马斯燃烧法结果普遍高于连续流动法结果,两种方法均具有良好的精密度和准确度。在提高检测效率、降低人员劳动强度和环境污染方面,杜马斯燃烧法优势明显。杜马斯燃烧法结果应用比值系数K(K=DN/LN)进行换算即可代替连续流动法结果。
Abstract
Aiming to improve efficiency of determination of total nitrogen in samples of reconstituted tobacco, a comparative study between Dumas combustion method (D method) and continuous flow method (L method) was carried out, and a preliminary investigation to use the results obtained by D method instead of those found by L method, through certain conversion, was also made. Good precision and accuracy were obtained by either of the 2 methods, and the results of total nitrogen found by the D method were generally higher. But on the whole, the D method had obvious advantages on having higher analytical efficiency, lower labouring intensity and less environmental pollution. It was shown that the results found by D method could be converted to values of L method by applying the ratio coefficient K (K=DN/LN).
中图分类号 O65 DOI 10.11973/lhjy-hx201807003
所属栏目 试验与研究
基金项目
收稿日期 2017/7/10
修改稿日期
网络出版日期
作者单位点击查看
备注周冰群,助理工程师,主要从事烟草质量分析研究
引用该论文: ZHOU Bingqun,WANG Xinhai,HOU Feng. Comparison between Dumas Combustion Method and Continuous Flow Method for Determination of Total Nitrogen in Reconstituted Tobacco[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2018, 54(7): 757~760
周冰群,王鑫海,侯峰. 杜马斯燃烧法与连续流动法测定再造烟叶中总氮量的比较[J]. 理化检验-化学分册, 2018, 54(7): 757~760
共有人对该论文发表了看法,其中:
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】张朝,葛少林,佘世科,等.连续流动法测定烟草中总氮含量的方法改进[J].广东化工, 2015,42(9):223-224.
【2】陈祖刚,蔡冰,王建新,等.国内外造纸法薄片工艺与品质比较[J].烟草科技, 2002(2):4-10.
【3】孙德平,徐建峰,刘良才,等.造纸法烟草薄片打浆工艺和助留助滤剂的研究[J].中华纸业, 2010,31(22):43-47.
【4】YC/T 161-2002烟草及烟草制品总氮的测定连续流动法[S].
【5】范志影,刘庆生,张萍.用凯氏法和杜马斯法测定植物样品中的全氮[J].现代科学仪器, 2007(1):46-47.
【6】郭晓旭,郭望山,任丽萍,等.饲料中硝态氮对燃烧法与凯氏法总氮含量测定结果的影响[J].中国畜牧杂志, 2008,44(21):49-52.
【7】AOAC Official Method 990.03 Protein (crude) in animal feed combustion method[S].
【8】GB 5009.5-2010食品安全国家标准食品中蛋白质的测定[S].
【9】GB/T 31578-2015粮油检验粮食及制品中粗蛋白测定杜马斯燃烧法[S].
【10】GB/T 24318-2009杜马斯燃烧法测定饲料原料中总氮含量及粗蛋白质的计算[S].
【11】NY/T 2007-2011谷类、豆类粗蛋白质含量的测定杜马斯燃烧法[S].
【12】SN/T 2115-2008进出口食品和饲料中总氮及粗蛋白的检测方法杜马斯燃烧法[S].
【13】孔浩辉,陈翠玲,王华.元素分析法快速测定烟草中的总氮[J].烟草科技, 2013(9):47-49.
【2】陈祖刚,蔡冰,王建新,等.国内外造纸法薄片工艺与品质比较[J].烟草科技, 2002(2):4-10.
【3】孙德平,徐建峰,刘良才,等.造纸法烟草薄片打浆工艺和助留助滤剂的研究[J].中华纸业, 2010,31(22):43-47.
【4】YC/T 161-2002烟草及烟草制品总氮的测定连续流动法[S].
【5】范志影,刘庆生,张萍.用凯氏法和杜马斯法测定植物样品中的全氮[J].现代科学仪器, 2007(1):46-47.
【6】郭晓旭,郭望山,任丽萍,等.饲料中硝态氮对燃烧法与凯氏法总氮含量测定结果的影响[J].中国畜牧杂志, 2008,44(21):49-52.
【7】AOAC Official Method 990.03 Protein (crude) in animal feed combustion method[S].
【8】GB 5009.5-2010食品安全国家标准食品中蛋白质的测定[S].
【9】GB/T 31578-2015粮油检验粮食及制品中粗蛋白测定杜马斯燃烧法[S].
【10】GB/T 24318-2009杜马斯燃烧法测定饲料原料中总氮含量及粗蛋白质的计算[S].
【11】NY/T 2007-2011谷类、豆类粗蛋白质含量的测定杜马斯燃烧法[S].
【12】SN/T 2115-2008进出口食品和饲料中总氮及粗蛋白的检测方法杜马斯燃烧法[S].
【13】孔浩辉,陈翠玲,王华.元素分析法快速测定烟草中的总氮[J].烟草科技, 2013(9):47-49.
相关信息