高效液相色谱法测定水产品中土霉素的残留量
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Abstract
中图分类号 O652.63 DOI 10.11973/lhjy-hx201811025
所属栏目 知识与经验
基金项目 广西重点研发项目（桂科AB16380252）
收稿日期 2018/1/17
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引用该论文: 黄鸾玉,杨姝丽,吴祥庆,韦信贤,童桂香,秦振发,黄玉柳,吴明媛. [J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2018, 54(11): 1355～1358
黄鸾玉,杨姝丽,吴祥庆,韦信贤,童桂香,秦振发,黄玉柳,吴明媛. 高效液相色谱法测定水产品中土霉素的残留量[J]. 理化检验－化学分册, 2018, 54(11): 1355～1358
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参考文献
【1】NEBOT C, GUARDDON M, SECO F, et al. Monitoring the presence of residues of tetracyclines in baby food samples by HPLC-MS/MS[J]. Food Control, 2014,46:495-501.
【2】张天姝,杨慧杰,孙世峰.饲料中4种四环素类药物的检测-高效液相色谱法[J].现代畜牧兽医, 2016(10):16-20.
【3】FRITZ J W, ZUO Y. Simultaneous determination of tetracycline, oxytetracycline, and 4-epitetracycline in milk by high-performance liquid chromatography[J]. Food Chemistry, 2007,105(3):1297-1301.
【4】37/2010/EU Commission regulation of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin[S].
【5】叶永丽,赫欣睿,高旭东,等.SPE-HPLC法检测早胜牛肉中土霉素、四环素和金霉素的残留[J].国际药学研究杂志, 2016,43(2):382-386.
【6】杨琳.动物性食品中土霉素、金霉素和四环素检测方法研究进展[J].中国动物检疫, 2012(8):63-66.
【7】NAGEL O G, BELTRAN M C, MOLINA M P, et al. Novel microbiological system for antibiotic detection in ovine milk[J]. Small Ruminant Research, 2012,102(1):26-31.
【8】DANG P K, DEGAND G, DANYI S, et al. Validation of a two-plate microbiological method for screening antibiotic residues in shrimp tissue[J]. Analytica Chimica Acta, 2010,672(1/2):30-39.
【9】YAN X D, HU X Z, ZHANG H C, et al. Direct determination of furaltadone metabolite, 3-amino-5-morpholinomethyl-2-oxazolidinone,in meats by a simple immunoassay[J]. Food and Agricultural Immunology, 2012,23(3):203-215.
【10】ZHOU Y, LI C Y, LI Y S, et al. Monoclonal antibody based inhibition ELISA as a new tool for the analysis of melamine in milk and pet food samples[J]. Food Chemistry, 2012,15(4):2681-2686.
【11】OKA H, ITO Y, MATSUMOTO H. Chromatographic analysis of tetracycline antibiotics in foods[J]. Journal of Chromatography A, 2000,882(1/2):109-133.
【12】MA T Y, VICKROY T W, SHIEN J H, et al. Improved nonaqueous capillary electrophoresis for tetracyclines at subparts per billion level[J]. Electrophoresis, 2012,33(11):1679-1682.
【13】JIAO Z, ZHANG S, CHEN H. Determination of tetracycline antibiotics in fatty food samples by selective pressurized liquid extraction coupled with high-performance liquid chromatography and tandem mass spectrometry[J]. Journal of Separation Science, 2015,38(1):73-80.
【14】于欢.动物可食性组织中兽药多残留检测关键技术研究[D].武汉:华中农业大学, 2010.
【15】ONAL A. Overview on liquid chromatographic analysis of tetracycline residues in food matrices[J]. Food Chemistry, 201l,127(1):197-203.
【16】ZHOU Q, ZHANG Y, WANG N, et al. Analysis of tetracyclines in chicken tissues and dung using LC-MS coupled with ultrasound-assisted enzymatic hydrolysis[J]. Food Control, 2014,46:324-331.
【17】洪武兴,孙良娟,刘益锋,等.液质联用法检测水产品中四环素类残留[J].现代食品科技, 2010,26(7):756-758.
【18】梅英杰,史新宇,董瑾,等.超高效液相色谱-串联质谱法同时检测鸡肉中氯霉素、四环素、金霉素和土霉素[J].食品与发酵工业, 2017,43(8):240-245.
【19】刘艳华,张纯萍,门立强,等.液相色谱-串联质谱法测定鸡肌肉组织中的四环素类药物残留[J].色谱, 2006,24(2):171-173.
【20】JIA F, WANG W, WANG J, et al. New strategy to enhance the extraction efficiency of pyrethroid pesticides in fish samples using a modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) method[J]. Anal Methods-UK, 2012,4(2):449-453.
【21】SC/T 3015-2002水产品中土霉素、四环素、金霉素残留量的测定[S].
【22】李慧芳.水产品中农、兽药残留检测样品前处理技术研究[D].烟台:烟台大学, 2012.
【23】PAROLO M E, SAVINI M C, VALLÉS J M, et al. Tetracycline adsorption on montmorillonite:pH and ionic strength effects[J]. Applied Clay Science, 2007,40(1):179-186.
【2】张天姝,杨慧杰,孙世峰.饲料中4种四环素类药物的检测-高效液相色谱法[J].现代畜牧兽医, 2016(10):16-20.
【3】FRITZ J W, ZUO Y. Simultaneous determination of tetracycline, oxytetracycline, and 4-epitetracycline in milk by high-performance liquid chromatography[J]. Food Chemistry, 2007,105(3):1297-1301.
【4】37/2010/EU Commission regulation of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin[S].
【5】叶永丽,赫欣睿,高旭东,等.SPE-HPLC法检测早胜牛肉中土霉素、四环素和金霉素的残留[J].国际药学研究杂志, 2016,43(2):382-386.
【6】杨琳.动物性食品中土霉素、金霉素和四环素检测方法研究进展[J].中国动物检疫, 2012(8):63-66.
【7】NAGEL O G, BELTRAN M C, MOLINA M P, et al. Novel microbiological system for antibiotic detection in ovine milk[J]. Small Ruminant Research, 2012,102(1):26-31.
【8】DANG P K, DEGAND G, DANYI S, et al. Validation of a two-plate microbiological method for screening antibiotic residues in shrimp tissue[J]. Analytica Chimica Acta, 2010,672(1/2):30-39.
【9】YAN X D, HU X Z, ZHANG H C, et al. Direct determination of furaltadone metabolite, 3-amino-5-morpholinomethyl-2-oxazolidinone,in meats by a simple immunoassay[J]. Food and Agricultural Immunology, 2012,23(3):203-215.
【10】ZHOU Y, LI C Y, LI Y S, et al. Monoclonal antibody based inhibition ELISA as a new tool for the analysis of melamine in milk and pet food samples[J]. Food Chemistry, 2012,15(4):2681-2686.
【11】OKA H, ITO Y, MATSUMOTO H. Chromatographic analysis of tetracycline antibiotics in foods[J]. Journal of Chromatography A, 2000,882(1/2):109-133.
【12】MA T Y, VICKROY T W, SHIEN J H, et al. Improved nonaqueous capillary electrophoresis for tetracyclines at subparts per billion level[J]. Electrophoresis, 2012,33(11):1679-1682.
【13】JIAO Z, ZHANG S, CHEN H. Determination of tetracycline antibiotics in fatty food samples by selective pressurized liquid extraction coupled with high-performance liquid chromatography and tandem mass spectrometry[J]. Journal of Separation Science, 2015,38(1):73-80.
【14】于欢.动物可食性组织中兽药多残留检测关键技术研究[D].武汉:华中农业大学, 2010.
【15】ONAL A. Overview on liquid chromatographic analysis of tetracycline residues in food matrices[J]. Food Chemistry, 201l,127(1):197-203.
【16】ZHOU Q, ZHANG Y, WANG N, et al. Analysis of tetracyclines in chicken tissues and dung using LC-MS coupled with ultrasound-assisted enzymatic hydrolysis[J]. Food Control, 2014,46:324-331.
【17】洪武兴,孙良娟,刘益锋,等.液质联用法检测水产品中四环素类残留[J].现代食品科技, 2010,26(7):756-758.
【18】梅英杰,史新宇,董瑾,等.超高效液相色谱-串联质谱法同时检测鸡肉中氯霉素、四环素、金霉素和土霉素[J].食品与发酵工业, 2017,43(8):240-245.
【19】刘艳华,张纯萍,门立强,等.液相色谱-串联质谱法测定鸡肌肉组织中的四环素类药物残留[J].色谱, 2006,24(2):171-173.
【20】JIA F, WANG W, WANG J, et al. New strategy to enhance the extraction efficiency of pyrethroid pesticides in fish samples using a modified QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) method[J]. Anal Methods-UK, 2012,4(2):449-453.
【21】SC/T 3015-2002水产品中土霉素、四环素、金霉素残留量的测定[S].
【22】李慧芳.水产品中农、兽药残留检测样品前处理技术研究[D].烟台:烟台大学, 2012.
【23】PAROLO M E, SAVINI M C, VALLÉS J M, et al. Tetracycline adsorption on montmorillonite:pH and ionic strength effects[J]. Applied Clay Science, 2007,40(1):179-186.
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