碳纤维材料残余应力的拉曼光谱试验
Raman Spectra Testing of Residual Stress in the Carbon Fiber Reinforced Composites
摘 要
研究了碳纤维布，碳纤维布浸渍胶单层和碳纤维布浸渍胶双层的拉曼光谱，测试了碳纤维布加热处理下的拉曼光谱，分析了温度对碳纤维布内应力的影响，同时测试了单轴压应力条件下的碳纤维布拉曼光谱。结果显示：碳纤维的D峰和G峰对浸渍固化、温度、外应力存在响应，可以用于探究碳纤维界面以及内部存在的残余应力，表明拉曼光谱可用于碳纤维及其复合材料的检测，在工业无损检测领域具有发展潜力。
拉曼光谱
残余应力
无损检测
carbon fiber
Raman spectra
residual stress
nondestructive testing
Abstract
The Raman spectra of the carbon fiber sheet, carbon fiber sheet/epoxy resin sheet, carbon fiber sheet/epoxy resin sheet/carbon fiber sheet were carried out. And the Raman spectra of carbon fiber sheet under high temperature and uniaxial stress were also carried out to explore the residual stress evolution. The testing results show that the Raman D mode and G mode are sensitive to the epoxy resin sheet solidification, temperature and uniaxial stress, and can be used to explore the interfacial residual stress between carbon fiber sheet and epoxy resin sheet. The Raman technology has the potential in the future nondestructive testing field.
中图分类号 TG115.28 DOI 10.11973/wsjc201908005
所属栏目 应力无损测试技术专题
基金项目 广东省自然科学基金博士启动项目资助（2018A030310001）；北京理工大学珠海学院校级科研基金项目资助（XK201803）
收稿日期 2019/5/10
修改稿日期
网络出版日期
作者单位点击查看
备注冯炎青(1988-),女,博士研究生,主要从事材料的拉曼物性研究
引用该论文: FENG Yanqing,SHEN Yang,YOU Yong. Raman Spectra Testing of Residual Stress in the Carbon Fiber Reinforced Composites[J]. Nondestructive Testing, 2019, 41(8): 20～23
冯炎青,沈洋,游泳. 碳纤维材料残余应力的拉曼光谱试验[J]. 无损检测, 2019, 41(8): 20～23
共有人对该论文发表了看法，其中：
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】CARLSSON L A, ADAMS D F, PIPES R B. Experimental characterization of advanced composite materials[J]. Polymer Reviews,2013,53(2):277-302.
【2】RAWAL S P. Metal-matrix composites for space applications[J]. Journal of the Minerals Metals & Materials Society, 2001, 53(4):14-17.
【3】LIU X Y, WANG W G, WANG D. Effect of nanometer TiC coated diamond on the strength and thermal conductivity of diamond/Al composites[J]. Mater. Chem. Phys., 2016, 182:256-262.
【4】FU H T, HUANG Y, WU H W, et al. Synthesis by vacuum infiltration, microstructure, and thermo-physical properties of graphite-aluminum composite[J]. Adv. Eng. Mater., 2016, 18:1609-1615.
【5】WANG J P, LINA M, XU Z, et al. Microstructure and mechanical properties of C/C-SiC composites fabricated by a rapid processing method[J]. Journal of the European Ceramic Society, 2009, 29:3091-3097.
【6】王春净,代云霏.碳纤维复合材料在航空领域的应用研究[J].机电产品开发与创新, 2010, 23(2):14-15.
【7】GUO M L. Study on hygrothermal ageing mechanisms of aerospace structure composites[J]. Aerospace Materials & Technology, 2002, 32(4):51-54.
【8】黄元.碳纤维增强环氧树脂基复合材料湿热残余应力的微Raman光谱测试表征[J].复合材料学报, 2009, 26(4):22-28.
【9】GANESAN S, MARADUDIN A A, MARADUDIN J. A lattice theory of morphic effects in crystals of the diamond structure[J]. Annals of Physics, 1970, 56(2):556-594.
【10】石彦平. 拉曼光谱研究碳纤维的微观结构和性能[D]. 上海:东华大学, 2011.
【11】KAO C C, YOUNG R J. A Raman spectroscopic investigation of heating effffects and the deformation behaviour of epoxy/SWNT composites[J]. Composites Science and Technology, 2004, 64:2291-2295.
【2】RAWAL S P. Metal-matrix composites for space applications[J]. Journal of the Minerals Metals & Materials Society, 2001, 53(4):14-17.
【3】LIU X Y, WANG W G, WANG D. Effect of nanometer TiC coated diamond on the strength and thermal conductivity of diamond/Al composites[J]. Mater. Chem. Phys., 2016, 182:256-262.
【4】FU H T, HUANG Y, WU H W, et al. Synthesis by vacuum infiltration, microstructure, and thermo-physical properties of graphite-aluminum composite[J]. Adv. Eng. Mater., 2016, 18:1609-1615.
【5】WANG J P, LINA M, XU Z, et al. Microstructure and mechanical properties of C/C-SiC composites fabricated by a rapid processing method[J]. Journal of the European Ceramic Society, 2009, 29:3091-3097.
【6】王春净,代云霏.碳纤维复合材料在航空领域的应用研究[J].机电产品开发与创新, 2010, 23(2):14-15.
【7】GUO M L. Study on hygrothermal ageing mechanisms of aerospace structure composites[J]. Aerospace Materials & Technology, 2002, 32(4):51-54.
【8】黄元.碳纤维增强环氧树脂基复合材料湿热残余应力的微Raman光谱测试表征[J].复合材料学报, 2009, 26(4):22-28.
【9】GANESAN S, MARADUDIN A A, MARADUDIN J. A lattice theory of morphic effects in crystals of the diamond structure[J]. Annals of Physics, 1970, 56(2):556-594.
【10】石彦平. 拉曼光谱研究碳纤维的微观结构和性能[D]. 上海:东华大学, 2011.
【11】KAO C C, YOUNG R J. A Raman spectroscopic investigation of heating effffects and the deformation behaviour of epoxy/SWNT composites[J]. Composites Science and Technology, 2004, 64:2291-2295.
相关信息
