固相萃取-离子色谱法测定血液中草甘膦及其代谢物氨甲基膦酸
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Abstract
中图分类号 O657.75 DOI 10.11973/lhjy-hx202003018
所属栏目 知识与经验
基金项目 贵州省教育厅青年科技人才成长项目（黔教合KY字[2018]285）；贵州警察学院自然科学青年项目（18QNZK01）
收稿日期 2019/7/22
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引用该论文: 赵志东,孟娇,张显强,王晓卉. [J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2020, 56(3): 349～351
赵志东,孟娇,张显强,王晓卉. 固相萃取-离子色谱法测定血液中草甘膦及其代谢物氨甲基膦酸[J]. 理化检验－化学分册, 2020, 56(3): 349～351
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参考文献
【1】DUKE S O, POWLES S B. Glyphosate:a once-in-a-century herbicide[J]. Pest Management Science, 2008,64(4):319-325.
【2】卢信,赵炳梓,张佳宝,等.除草剂草甘膦的性质及环境行为综述[J].土壤通报, 2005,36(5):785-790.
【3】何凯,李国芳,吴柱东,等.草甘膦分析方法的研究进展[J].理化检验-化学分册, 2011,47(8):991-995.
【4】KOLLER V J, FVRHACKER M, NERSESYAN A, et al. Cytotoxic and DNA-damaging properties of glyphosate and Roundup in human-derived buccal epithelial cells[J]. Archives of Toxicology, 2012,86(5):805-813.
【5】MESNAGE R, BERNAY B, SÉRALINI G E. Ethoxylated adjuvants of glyphosate-based herbicides are active principles of human cell toxicity[J]. Toxicology, 2013,313(2/3):122-128.
【6】汪海萍,邵燕,王志良,等.分光光度法测定废水中草甘膦的探讨[J].环境监测管理与技术, 2012,24(3):56-59.
【7】吴淑彬,刘国红,王欣茹,等.紫外分光光度法检测血清草甘膦中毒方法的建立和应用[J].国际检验医学杂志, 2014,35(8):1024-1025.
【8】王敏,李广益,高慧,等.高效液相色谱-柱后衍生法测定水中草甘膦[J].食品科技, 2017,42(2):295-297.
【9】NEDELKOSKA T V, LOW GK C. High-performance liquid chromatographic determination of glyphosate in water and plant material after pre-column derivatisation with 9-fluorenylmethyl chloroformate[J]. Analytica Chimica Acta, 2004,511(1):145-153.
【10】SUN L S, KONG D Y, GU W D, et al. Determination of glyphosate in soil/sludge by high performance liquid chromatography[J]. Journal of Chromatography A, 2017,1502:8-13.
【11】ZHANG Y Y, ZHANG Y, QU Q S, et al. Determination of glyphosate and aminomethylphosphonic acid in soybean samples by high performance liquid chromatography using a novel fluorescent labeling reagent[J]. Analytical Methods, 2013,5(22):64-65.
【12】王勇,吴波,连厚彬,等.离子色谱法检验尸体心血中草甘膦[J].色谱, 2012,30(4):419-422.
【13】朱惠扬,李晓晶,甘平胜,等.离子色谱法同时测定水源水和饮用水中草甘膦和氨甲基膦酸[J].中国卫生检验杂志, 2016,26(10):1396-1397.
【14】ZHU Y, ZHANG F F, TONG C L, et al. Determination of glyphosate by ion chromatography[J]. Journal of Chromatography A, 1999,850(1/2):297-301.
【15】潘丽萍,张锋,刘庆东,等.气相色谱联用质谱法同时检测人体尿液中草甘膦及氨甲基膦酸含量[J].中国工业医学杂志, 2016,29(1):36-40.
【16】何龙凉,陈延伟,陈智鹏,等.气相色谱-串联质谱法测定不同原产国抗草甘膦转基因大豆中草甘膦及其代谢物的残留量[J].食品安全质量检测学报, 2016,7(9):3481-3486.
【17】成婧,王美玲,龚强,等.液相色谱-串联质谱法检测植物源食品中草甘膦及其代谢物的残留量[J].食品安全质量检测学报, 2016,7(1):138-144.
【18】张燕,舒平,陆敏,等.分散固相萃取/衍生化-高效液相色谱-串联质谱法同时测定水和食品中草甘膦、草铵膦和氨甲基膦酸残留[J].食品安全质量检测学报, 2017,8(4):346-352.
【19】MARTINS-JUNIOR H A, LEBRE D T, WANG A Y, et al. An alternative and fast method for determination of glyphosate and aminomethylphosphonic acid (AMPA) residues in soybean using liquid chromatography coupled with tandem mass spectrometry[J]. Rapid Communications in Mass Spectrometry, 2009,23(7):1029-1034.
【20】JENSEN P K, WUJCIK C E, MCGUIRE M K, et al. Validation of reliable and selective methods for direct determination of glyphosate and aminomethylphosphonic acid in milk and urine using LC-MS/MS[J]. Journal of Environmental Science and Health, Part B, 2016,51(4):254-259.
【2】卢信,赵炳梓,张佳宝,等.除草剂草甘膦的性质及环境行为综述[J].土壤通报, 2005,36(5):785-790.
【3】何凯,李国芳,吴柱东,等.草甘膦分析方法的研究进展[J].理化检验-化学分册, 2011,47(8):991-995.
【4】KOLLER V J, FVRHACKER M, NERSESYAN A, et al. Cytotoxic and DNA-damaging properties of glyphosate and Roundup in human-derived buccal epithelial cells[J]. Archives of Toxicology, 2012,86(5):805-813.
【5】MESNAGE R, BERNAY B, SÉRALINI G E. Ethoxylated adjuvants of glyphosate-based herbicides are active principles of human cell toxicity[J]. Toxicology, 2013,313(2/3):122-128.
【6】汪海萍,邵燕,王志良,等.分光光度法测定废水中草甘膦的探讨[J].环境监测管理与技术, 2012,24(3):56-59.
【7】吴淑彬,刘国红,王欣茹,等.紫外分光光度法检测血清草甘膦中毒方法的建立和应用[J].国际检验医学杂志, 2014,35(8):1024-1025.
【8】王敏,李广益,高慧,等.高效液相色谱-柱后衍生法测定水中草甘膦[J].食品科技, 2017,42(2):295-297.
【9】NEDELKOSKA T V, LOW GK C. High-performance liquid chromatographic determination of glyphosate in water and plant material after pre-column derivatisation with 9-fluorenylmethyl chloroformate[J]. Analytica Chimica Acta, 2004,511(1):145-153.
【10】SUN L S, KONG D Y, GU W D, et al. Determination of glyphosate in soil/sludge by high performance liquid chromatography[J]. Journal of Chromatography A, 2017,1502:8-13.
【11】ZHANG Y Y, ZHANG Y, QU Q S, et al. Determination of glyphosate and aminomethylphosphonic acid in soybean samples by high performance liquid chromatography using a novel fluorescent labeling reagent[J]. Analytical Methods, 2013,5(22):64-65.
【12】王勇,吴波,连厚彬,等.离子色谱法检验尸体心血中草甘膦[J].色谱, 2012,30(4):419-422.
【13】朱惠扬,李晓晶,甘平胜,等.离子色谱法同时测定水源水和饮用水中草甘膦和氨甲基膦酸[J].中国卫生检验杂志, 2016,26(10):1396-1397.
【14】ZHU Y, ZHANG F F, TONG C L, et al. Determination of glyphosate by ion chromatography[J]. Journal of Chromatography A, 1999,850(1/2):297-301.
【15】潘丽萍,张锋,刘庆东,等.气相色谱联用质谱法同时检测人体尿液中草甘膦及氨甲基膦酸含量[J].中国工业医学杂志, 2016,29(1):36-40.
【16】何龙凉,陈延伟,陈智鹏,等.气相色谱-串联质谱法测定不同原产国抗草甘膦转基因大豆中草甘膦及其代谢物的残留量[J].食品安全质量检测学报, 2016,7(9):3481-3486.
【17】成婧,王美玲,龚强,等.液相色谱-串联质谱法检测植物源食品中草甘膦及其代谢物的残留量[J].食品安全质量检测学报, 2016,7(1):138-144.
【18】张燕,舒平,陆敏,等.分散固相萃取/衍生化-高效液相色谱-串联质谱法同时测定水和食品中草甘膦、草铵膦和氨甲基膦酸残留[J].食品安全质量检测学报, 2017,8(4):346-352.
【19】MARTINS-JUNIOR H A, LEBRE D T, WANG A Y, et al. An alternative and fast method for determination of glyphosate and aminomethylphosphonic acid (AMPA) residues in soybean using liquid chromatography coupled with tandem mass spectrometry[J]. Rapid Communications in Mass Spectrometry, 2009,23(7):1029-1034.
【20】JENSEN P K, WUJCIK C E, MCGUIRE M K, et al. Validation of reliable and selective methods for direct determination of glyphosate and aminomethylphosphonic acid in milk and urine using LC-MS/MS[J]. Journal of Environmental Science and Health, Part B, 2016,51(4):254-259.
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