Preparation Process Parameters of Proficiency Testing Sample for Guarded Hot Plate Apparatus Thermal Conductivity
摘 要
研究了动态水热反应过程中硅钙比、反应温度、反应时间、水固比和均化速率等工艺参数对硬硅钙石料浆的影响规律,确定了硅钙比、反应温度、反应时间、水固比和均化速率等工艺参数。在该工艺参数下制备防护热板法导热系数能力验证样品,并对其均匀性和稳定性进行检验。结果表明:用此参数制备的样品的均匀性和稳定性都符合能力验证样品的要求,该样品可用于评估试验室防护热板法导热系数的检测能力。
Abstract
The effects of process parameters such as silicon-calcium ratio, reaction temperature, reaction time, water-solid ratio and homogenization speed on the xonotlite slurry during dynamic hydrothermal reaction were studied. The process parameters such as silicon-calcium ratio, reaction temperature, reaction time, water-solid ratio and homogenization speed were determined. The proficiency testing sample of guarded hot plate apparatus thermal conductivity were prepared with the preparation process parameters, and the uniformity and stability were tested. The results show that the uniformity and stability of the sample prepared by this paramenter meet the requirements of the proficiency testing sample, which can be used to evaluate the test ability of guarded hot plate apparatus thermal conductivity in laboratory.
中图分类号 TB332 TQ320.77 DOI 10.11973/lhjy-wl202008002
所属栏目 试验与研究
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收稿日期 2020/3/10
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备注凡丽梅(1983-),女,硕士,主要从事材料热学性能检测和无损检测表征技术的研究,limei8729@126.com
引用该论文: FAN Limei,ZHANG Xia,WANG Congke,DONG Fangxu,ZHAO Fubao,ZHENG Suping. Preparation Process Parameters of Proficiency Testing Sample for Guarded Hot Plate Apparatus Thermal Conductivity[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2020, 56(8): 5~12
凡丽梅,张霞,王从科,董方旭,赵付宝,郑素萍. 热防护板法导热系数能力验证样品的制备工艺参数[J]. 理化检验-物理分册, 2020, 56(8): 5~12
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【3】肖鑫,张鹏.泡沫石墨/石蜡复合相变材料热物性研究[J].工程热物理学报,2013,34(3):530-533.
【4】蒋运运,张玉忠,郑水林.复合相变材料的制备与应用研究进展[J].中国非金属矿工业导刊,2011(3):4-7.
【5】陈洪亮.热防护板法检测绝热材料导热系数[J].节能环保,2015(19):597-599.
【6】索亚运,李艳宁.防护热板法高温高热系数测定仪关键技术研究[D].天津:天津大学,2015.
【7】SCOARNEC V,HAMEURY J,HAY B. A new guarded hot desiged for thermal-conductivity measurements at high temperature[J]. International Journal of Thermophysics,2015,36(2):540-556.
【8】苏高辉,杨自春,孙丰瑞.硅薄膜导热系数微尺度效应的临界尺寸[J].纳米技术与精密工程,2014,12(3):176-181.
【9】GOYAL V BALANDIN A A. Thermal properties of the hybrid graphene-metal nano-micro-composites:Applications in thermal interface materials[J]. Applied Physics Letters,2012,7:73-79.
【10】索亚运,李艳宁.防护热板法快速测量物质导热系数[J].纳米技术与精密工程,2017,15(3):193-198.
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