搜索热:失效分析 陶瓷
扫一扫 加微信
首页 > 期刊论文 > 论文摘要
基体偏压对磁控溅射制备CrAlN纳米多层薄膜微观结构和力学性能的影响
          
Influence of Substrate Bias Voltage on Microstructure and MechanicalProperties of CrAlN Nano-mutilayer Film Prepared by Magnetron Sputtering

摘    要
采用磁控溅射技术在不同基体偏压(-60,-70,-80,-90 V)下制备了CrAlN纳米多层薄膜,研究了基体偏压对薄膜微观结构和力学性能的影响。结果表明:随着基体偏压绝对值增大,CrAlN纳米多层薄膜中的氮含量增加,物相组成不变,择优取向由CrN(111)晶面转变为CrN(200)晶面,薄膜表面孔隙减少,组织致密性得到改善;基体偏压为-60~-80 V时,偏压对薄膜沉积速率的影响较小,偏压绝对值大于80 V时,沉积速率明显下降;随着基体偏压绝对值增大,薄膜的硬度和弹性模量提高,膜基结合力先增大后减小,在偏压为-80 V时达到最大。
标    签 CrAlN纳米多层薄膜   磁控溅射   基体偏压   微观结构   力学性能   CrAlN nano-multilayer film   magnetron sputtering   substrate bias voltage   microstructure   mechanical property  
 
Abstract
CrAlN nano-multilayer films were prepared by magnetron sputtering technique under different bias voltages (-60,-70,-80,-90 V) of the substrate, and the effect of bias voltage of the substrate on the microstructure and mechanical properties of the film was studied. The results show that with increasing absolute value of the substrate bias voltage, the nitrogen content in the CrAlN nano-multilayer film increased, the phase composition unchanged, the preferred orientation changed from the CrN (111) crystal plane to the CrN (200) crystal plane, the pores on the film surface decreased, and the densification of microstructure was improved. When the bias voltage of the substrate was between -60 and -80 V, the bias voltage had little effect on the film deposition rate. When absolute value of the bias voltage was higher than 80 V, the deposition rate decreased significantly. With increasing absolute value of bias voltage of the substrate, the hardness and elastic modulus of the film increased, and the film base bonding force increased and then decreased, reaching the maximum at -80 V of bias voltage.

中图分类号 TG174   DOI 10.11973/jxgccl202103008

 
  中国光学期刊网论文下载说明


所属栏目 试验研究

基金项目 浙江省自然科学基金资助项目(Y15E050060)

收稿日期 2020/4/13

修改稿日期 2021/1/6

网络出版日期

作者单位点击查看

备注王宇星(1984-),男,浙江衢州人,副教授,博士

引用该论文: WANG Yuxing,ZHANG Xia. Influence of Substrate Bias Voltage on Microstructure and MechanicalProperties of CrAlN Nano-mutilayer Film Prepared by Magnetron Sputtering[J]. Materials for mechancial engineering, 2021, 45(3): 41~45
王宇星,张侠. 基体偏压对磁控溅射制备CrAlN纳米多层薄膜微观结构和力学性能的影响[J]. 机械工程材料, 2021, 45(3): 41~45


论文评价
共有人对该论文发表了看法,其中:
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
分享论文
分享到新浪微博 分享到腾讯微博 分享到人人网 分享到 Google Reader 分享到百度搜藏分享到Twitter

参考文献
【1】董文杰,张钧,孙宇菲,等.CrN系硬质膜的发展与应用[J].材料保护,2019,52(12):129-134. DONG W J, ZHANG J, SUN Y F, et al. Development and application of CrN-based hard films[J]. Materials Protection, 2019, 52(12):129-134.
 
【2】谈淑咏,张旭海,吴湘君,等.氮流量比对直流反应磁控溅射制备氮化铬涂层组织和性能的影响[J].机械工程材料,2010,34(7):34-37. TAN S Y, ZHANG X H, WU X J, et al. Effect of N2 flow rate on structure and property of CrN coatings deposited by DC reactive magnetron sputtering[J]. Materials for Mechancial Engineering, 2010, 34(7):34-37.
 
【3】王翠凤,邱锡荣,康爱军,等.S136不锈钢基体溅射氮化铬薄膜的硬度和接触角[J].机械工程材料,2013,37(12):21-26. WANG C F, QIU X R, KANG A J, et al, Hardness and contact angle of CrN coating sputtered on matrix of S136 stainless steels[J]. Materials for Mechancial Engineering, 2013, 37(12):21-26.
 
【4】楼白杨,王宇星.Mo含量对CrMoAlN薄膜微观结构和摩擦磨损性能的影响[J].金属学报,2016,52(6):727-733. LOU B Y, WANG Y X.Effects of Mo content on the micro-structure and tribological properties of CrMoAlN films[J]. Acta Metallurgica Sinica, 2016, 52(6):727-733.
 
【5】余春燕.闭合场非平衡磁控溅射沉积的CrAlN薄膜组织结构和性能研究[D].太原:太原理工大学,2009. YU C Y. Study on microstructure and properties of CrAlN coatings deposited by closed field unbalanced megnetron sputtering[D]. Taiyuan:Taiyuan University of Technology, 2009.
 
【6】BARDI U,CHENAKIN S P,GHEZZI F,et al.High-temperature oxidation of CrN/AlN multilayer coatings[J].Applied Surface Science,2005,252(5):1339-1349.
 
【7】LIN J L,MOORE J J,WANG J,et al.High temperature oxidation behavior of CrN/AlN superlattice films[J].Thin Solid Films,2011,519(8):2402-2408.
 
【8】LIN J L,ZHANG N,WU Z L,et al.Thick CrN/AlN superlattice coatings deposited by the hybrid modulated pulsed power and pulsed dc magnetron sputtering[J].Surface and Coatings Technology,2013,228(S1):601-606.
 
【9】CABRERA G,CAICEDO J C,AMAYA C,et al.Enhancement of mechanical and tribological properties in AISI D3 steel substrates by using a non-isostructural CrN/AlN multilayer coating[J].Materials Chemistry and Physics,2011,125(3):576-586.
 
相关信息
   标题 相关频次
 Ti(C,N)含量对无压烧结Ti(C,N)/ZrO2陶瓷复合材料微观结构和性能的影响
 4
 TiC含量对无压烧结TiC/ZrO2导电陶瓷复合材料微观结构和性能的影响
 4
 TiC含量对无压烧结TiC-Al2O3导电陶瓷复合材料微观结构与性能的影响
 4
 磁控溅射制备Al-Cu合金薄膜的纳米压痕力学性能与强化机制
 4
 电流辅助累积叠轧镁/铝层状复合板的微观形貌及力学性能
 4
 芳纶纤维增强尼龙6复合材料的制备与性能
 4
 环氧泡沫材料的力学性能及微观结构
 4
 溅射工艺参数对TiAlN薄膜力学性能及结构成分的影响
 4
 脉冲射流电铸纳米晶铜的组织与性能
 4
 射流电铸快速成型纳米晶铜的组织与性能
 4
 06Cr19Ni10不锈钢/A283低碳钢扩散焊接接头的显微组织和力学性能
 3
 06Cr20Ni11钢埋弧焊焊缝的显微组织和性能
 3
 1060铝在累积轧制中组织和性能的演变
 3
 10Ni5CrMoV钢MAG焊接接头的显微组织与力学性能
 3
 12Cr13钢预热处理工艺参数优化
 3
 12Cr1MoV钢过热器爆管的显微组织和力学性能
 3
 16Mo3钢大直径大变形量试制中频弯管的组织与性能
 3
 2024铝合金电子束焊接接头的显微组织与力学性能
 3
 20Cr钢与B级钢焊接接头的组织和性能
 3
 2205双相不锈钢/Q345低合金钢爆炸复合板的组织与力学性能
 3
 240 MPa级高强IF钢的冷轧压下率和退火温度
 3
 300 MW机组锁口叶片断裂原因分析
 3
 3003铝合金无缝管制备过程中的显微组织与力学性能变化
 3
 3D打印18Ni300模具钢的显微组织及力学性能
 3
 5 mm厚6005A-T6铝合金双轴肩搅拌摩擦焊接头的组织及性能
 3
 5 mm厚6082-T6铝合金双轴肩搅拌摩擦焊接头的组织与性能
 3
 5083/6063不等厚铝合金双丝CMT角焊接头的组织与性能
 3
 550 MPa级高强度高延性汽车方管用钢的显微组织与力学性能
 3
 600 MPa级热轧双相钢的动态连续冷却转变行为及其热轧卷取工艺的优化
 3
 600 MW机组次末级叶片断裂原因分析
 3