Causes and Solutions of Pseudo Shift of Diffraction Peak in Short Wavelength Characteristic X-ray Diffraction
摘 要
利用短波长特征X射线衍射仪对样品进行应力测试,测试样品表面附近的衍射峰时发现,衍射角明显偏离理论衍射角。通过理论和试验对该衍射峰赝偏移的原因进行了分析,并提出了解决措施。结果表明:由于短波长特征X射线波长短、衍射角小,入射准直器和接收准直器形成的规范体积截面为长菱形,当样品未充满规范体积时,导致衍射峰赝偏移,进而造成衍射角测试存在误差,影响应变计算结果的准确性。可通过减小准直器宽度、采用高角度衍射峰、使用对称法、翻转样品及应用理想参考样品等方法降低衍射峰赝偏移对应变计算结果的影响。
Abstract
The stress of the sample was measured by short wavelength characteristic X-ray diffractometer. It was found that the diffraction angle obviously deviated from the theoretical diffraction angle during test the diffraction peak near the sample surface. The reason for pseudo migration of diffraction peak was analyzed by theory and experiment, and the solutions were put forward. The results show that due to the wave length of the short wavelength characteristic X-ray was short and the diffraction angle was small, the gauge volume cross section formed by the incident collimator and the receiving collimator was a long diamond. When the sample was not filled with the gauge volume, leading to the pseudo shift of diffraction peak, resulting in the error of the diffraction angle measurement and affecting the accuracy of strain calculated results. The influence of pseudo shift of diffraction peak on strain calculated results could be reduced by reducing the width of collimator, using high angle diffraction peak, using symmetry method, turning sample and using ideal reference sample.
中图分类号 TG115.22 DOI 10.11973/lhjy-wl202109001
所属栏目 试验与研究
基金项目
收稿日期 2020/11/11
修改稿日期
网络出版日期
作者单位点击查看
备注窦世涛(1988-),男,高级工程师,主要从事内部残余应力无损检测分析及仪器的开发研究工作,doushitao@126.com
引用该论文: DOU Shitao,ZHENG Lin,ZHANG Jin,ZHANG Lunwu,ZHAO Fangchao,LIAN Yong,CHEN Xin,JI Pengfei,XU Weisheng. Causes and Solutions of Pseudo Shift of Diffraction Peak in Short Wavelength Characteristic X-ray Diffraction[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2021, 57(9): 1~4
窦世涛,郑林,张津,张伦武,赵方超,连勇,陈新,计鹏飞,徐伟生. 短波长特征X射线衍射的衍射峰赝偏移现象的产生原因及解决措施[J]. 理化检验-物理分册, 2021, 57(9): 1~4
共有人对该论文发表了看法,其中:
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】郑林, 何长光, 彭正坤.短波长X射线衍射测量装置和方法:中国CN200410068880. 2[P].2004-07-14.
【2】肖勇, 郑林, 窦世涛, 等.短波长特征X射线衍射法无损测定孔挤压强化A100钢内部径向残余应力分布[J].理化检验(物理分册), 2016, 52(8):548-551.
【3】窦世涛, 郑林, 张朝晖, 等.短波长X射线衍射法测试纳米铝块体的内部残余应力[J].机械工程材料, 2016, 40(9):97-100.
【4】郑林, 车路长, 张津, 等.预拉伸厚铝板内部残余应力与晶粒取向均匀性的研究[J].精密成形工程, 2014, 6(5):50-58.
【5】计鹏飞, 张津, 郑林, 等.转速对7075-T651铝合金搅拌摩擦焊接件内部残余应力分布的影响[J].精密成形工程, 2016, 8(4):8-15.
【6】郑林, 窦世涛, 张津, 等.短波长X射线衍射技术及在环境工程中的应用展望[J].装备环境工程, 2017, 14(6):43-48.
【7】JI P F, ZHANG J, ZHENG L, et al.Comparison of residual stress determination using different crystal planes by short-wavelength X-ray diffraction in a friction-stir-welded aluminum alloy plate[J].Journal of Materials Science, 2017, 52(21):12834-12847.
【8】杨中玉, 牛关梅, 曹海龙, 等.7050和7075铝合金板材的淬火残余应力[J].理化检验(物理分册), 2019, 55(1):9-14.
【9】韩雨辰, 朱文龙, 姜传海.复合喷丸对铝-铜-镁合金表面形貌和硬度的影响[J].理化检验(物理分册), 2021, 57(5):6-9.
【10】ALLEN A J, HUTCHINGS M T, WINDSOR C G, et al.Neutron diffraction methods for the study of residual stress fields[J].Advances in Physics, 1985, 34(4):445-473.
【11】REIMERS W, BRODA M, BRUSCH G, et al.Evaluation of residual stresses in the bulk of materials by high energy synchrotron diffraction[J].Journal of Nondestructive Evaluation, 1998, 17(3):129-140.
【12】PARADOWSKA A M, PRICE J W H, FINLAYSON T R, et al.Comparison of neutron and synchrotron diffraction measurements of residual stress in bead-on-plate weldments[J].Journal of Pressure Vessel Technology, 2010, 132(1):011502.
【13】REIMERS W, PYZALLA A, BRODA M, et al.The use of high-energy synchrotron diffraction for residual stress analyses[J].Journal of Materials Science Letters, 1999, 18(7):581-583.
【14】蒋文春, WOO W, 王炳英, 等.中子衍射和有限元法研究不锈钢复合板补焊残余应力[J].金属学报, 2012, 48(12):1525-1529.
【2】肖勇, 郑林, 窦世涛, 等.短波长特征X射线衍射法无损测定孔挤压强化A100钢内部径向残余应力分布[J].理化检验(物理分册), 2016, 52(8):548-551.
【3】窦世涛, 郑林, 张朝晖, 等.短波长X射线衍射法测试纳米铝块体的内部残余应力[J].机械工程材料, 2016, 40(9):97-100.
【4】郑林, 车路长, 张津, 等.预拉伸厚铝板内部残余应力与晶粒取向均匀性的研究[J].精密成形工程, 2014, 6(5):50-58.
【5】计鹏飞, 张津, 郑林, 等.转速对7075-T651铝合金搅拌摩擦焊接件内部残余应力分布的影响[J].精密成形工程, 2016, 8(4):8-15.
【6】郑林, 窦世涛, 张津, 等.短波长X射线衍射技术及在环境工程中的应用展望[J].装备环境工程, 2017, 14(6):43-48.
【7】JI P F, ZHANG J, ZHENG L, et al.Comparison of residual stress determination using different crystal planes by short-wavelength X-ray diffraction in a friction-stir-welded aluminum alloy plate[J].Journal of Materials Science, 2017, 52(21):12834-12847.
【8】杨中玉, 牛关梅, 曹海龙, 等.7050和7075铝合金板材的淬火残余应力[J].理化检验(物理分册), 2019, 55(1):9-14.
【9】韩雨辰, 朱文龙, 姜传海.复合喷丸对铝-铜-镁合金表面形貌和硬度的影响[J].理化检验(物理分册), 2021, 57(5):6-9.
【10】ALLEN A J, HUTCHINGS M T, WINDSOR C G, et al.Neutron diffraction methods for the study of residual stress fields[J].Advances in Physics, 1985, 34(4):445-473.
【11】REIMERS W, BRODA M, BRUSCH G, et al.Evaluation of residual stresses in the bulk of materials by high energy synchrotron diffraction[J].Journal of Nondestructive Evaluation, 1998, 17(3):129-140.
【12】PARADOWSKA A M, PRICE J W H, FINLAYSON T R, et al.Comparison of neutron and synchrotron diffraction measurements of residual stress in bead-on-plate weldments[J].Journal of Pressure Vessel Technology, 2010, 132(1):011502.
【13】REIMERS W, PYZALLA A, BRODA M, et al.The use of high-energy synchrotron diffraction for residual stress analyses[J].Journal of Materials Science Letters, 1999, 18(7):581-583.
【14】蒋文春, WOO W, 王炳英, 等.中子衍射和有限元法研究不锈钢复合板补焊残余应力[J].金属学报, 2012, 48(12):1525-1529.
相关信息