取向硅钢超大高斯晶粒取向偏离角的X射线衍射测量
X-ray diffraction measurement of orientation deviation angle of super-large Gaussian grain in oriented silicon steel
摘 要
介绍了一种适用于超大晶粒取向硅钢的高斯晶粒取向偏离角的X射线衍射测量方法，提出了将试探法和探测器扫描法相结合的方式进行测量。结果表明：该方法可以同时获得准确的实际衍射角度和取向偏离角度，试样制备方式简单，对设备的要求低且测量结果准确。
高斯晶粒取向
偏离角
X射线衍射
oriented silicon steel
Gaussian grain orientation
deviation angle
X-ray diffraction
Abstract
This paper introduces a X-ray diffraction measurement method of Gaussian grain orientation deviation angle for ultra-large grain oriented silicon steel, and puts forward a method of combining the test method with the detector scanning. The results show that this method can obtain accurate actual diffraction angle and orientation deviation angle at the same time. The sample preparation method is simple, the requirements for equipment are low, and the measurement results are accurate.
中图分类号 TG113 DOI 10.11973/lhjy-wl202202009
所属栏目 试验与研究
基金项目 国家自然科学基金资助项目(51761033)
收稿日期 2021/3/14
修改稿日期
网络出版日期
作者单位点击查看
备注林子博(1997-)，男，硕士研究生，主要从事硅钢生产工艺的研究工作
引用该论文: LIN Zibo,LIU Jianhui,WU Zhongwang,LI Yiming,JIN Zili. X-ray diffraction measurement of orientation deviation angle of super-large Gaussian grain in oriented silicon steel[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2022, 58(2): 36～39
林子博,刘建辉,吴忠旺,李一鸣,金自力. 取向硅钢超大高斯晶粒取向偏离角的X射线衍射测量[J]. 理化检验－物理分册, 2022, 58(2): 36～39
共有人对该论文发表了看法，其中：
人认为该论文很差
人认为该论文较差
人认为该论文一般
人认为该论文较好
人认为该论文很好
参考文献
【1】QUONDAM A S,RIGANTI F F,LAUDANI A,et al.An effective neural network approach to reproduce magnetic hysteresis in electrical steel under arbitrary excitation waveforms[J].Journal of Magnetism and Magnetic Materials,2021,528:167735.
【2】夏彬,韩松,张楠,等.硅钢的研究现状及发展趋势[J].中国冶金,2018,28(6):9-12.
【3】曹树卫,申勇,孙江美.浅析电工钢的生产现状及技术发展[J].轧钢,2008,25(5):35-38.
【4】ZHANG B,MENG L,MA G,et al.Twinning behavior in cold-rolling ultra-thin grain-oriented silicon steel[J].Crystals,2021,11(2):187.
【5】YUAN C,GAO X X,LI J H,et al.Secondary recrystallization of Goss texture in magnetostrictive Fe-Ga-based sheets[J].Rare Metals,2020,39(11):1288-1294.
【6】HE Z H,SHA Y H,SHAN N,et al.Secondary recrystallization goss texture development in a binary Fe81Ga19 sheet induced by inherent grain boundary mobility[J].Metals,2019,9(12):1254.
【7】张静,李莉,贾志伟,等.不同工艺下取向硅钢超薄带中Goss织构取向分析[J].材料热处理学报,2020,41(10):80-85.
【8】刘刚,王福,苏雷,等.蚀坑法求算取向硅钢再结晶织构的ODF[J].东北大学学报,1997,18(6):37-40.
【9】刘竞艳,李鹏,苗壮,等.两种测定难熔单晶晶面偏离角方法的对比[J].理化检验(物理分册),2016,52(1):17-20.
【10】DING Z,PASCAL E,DE G M.Indexing of electron back-scatter diffraction patterns using a convolutional neural network[J].Acta Materialia,2020,199:370-382.
【11】KIM S H,YANG M,LEE H Y,et al.Structural characteristics of α-Ga2O3 films grown on sapphire by halide vapor phase epitaxy[J].Materials Science in Semiconductor Processing,2021,123:105534.
【12】刘涛,毛卫民,冯惠平,等.用X射线透射法测量热轧铝板整体织构[J].物理测试,2005,23(4):11-14.
【13】WU X Y,SUO H L,LI J Z,et al. In situ EBSD study on the microstructural transformation of the Ni5W substrate for coated conductors[J].Microscopy and Microanalysis,2021,27(1):36-43.
【14】方建锋,田志凌,秦英,等.取向硅钢[001]晶向分布的非对称X射线衍射法测定[J].钢铁研究学报,2008,20(5):48-51.
【15】胡建民,王蕊,王春婷,等.晶体X射线衍射模型和布拉格方程的一般推导[J].大学物理,2015,34(3):1-2.
【16】李赛.超薄无取向硅钢研发[D].呼和浩特:内蒙古工业大学,2020.
【17】崔凤娥,杨平,毛卫民.取向硅钢中高斯晶粒异常长大选择性行为[J].北京科技大学学报,2010,32(9):1157-1162.
【2】夏彬,韩松,张楠,等.硅钢的研究现状及发展趋势[J].中国冶金,2018,28(6):9-12.
【3】曹树卫,申勇,孙江美.浅析电工钢的生产现状及技术发展[J].轧钢,2008,25(5):35-38.
【4】ZHANG B,MENG L,MA G,et al.Twinning behavior in cold-rolling ultra-thin grain-oriented silicon steel[J].Crystals,2021,11(2):187.
【5】YUAN C,GAO X X,LI J H,et al.Secondary recrystallization of Goss texture in magnetostrictive Fe-Ga-based sheets[J].Rare Metals,2020,39(11):1288-1294.
【6】HE Z H,SHA Y H,SHAN N,et al.Secondary recrystallization goss texture development in a binary Fe81Ga19 sheet induced by inherent grain boundary mobility[J].Metals,2019,9(12):1254.
【7】张静,李莉,贾志伟,等.不同工艺下取向硅钢超薄带中Goss织构取向分析[J].材料热处理学报,2020,41(10):80-85.
【8】刘刚,王福,苏雷,等.蚀坑法求算取向硅钢再结晶织构的ODF[J].东北大学学报,1997,18(6):37-40.
【9】刘竞艳,李鹏,苗壮,等.两种测定难熔单晶晶面偏离角方法的对比[J].理化检验(物理分册),2016,52(1):17-20.
【10】DING Z,PASCAL E,DE G M.Indexing of electron back-scatter diffraction patterns using a convolutional neural network[J].Acta Materialia,2020,199:370-382.
【11】KIM S H,YANG M,LEE H Y,et al.Structural characteristics of α-Ga2O3 films grown on sapphire by halide vapor phase epitaxy[J].Materials Science in Semiconductor Processing,2021,123:105534.
【12】刘涛,毛卫民,冯惠平,等.用X射线透射法测量热轧铝板整体织构[J].物理测试,2005,23(4):11-14.
【13】WU X Y,SUO H L,LI J Z,et al. In situ EBSD study on the microstructural transformation of the Ni5W substrate for coated conductors[J].Microscopy and Microanalysis,2021,27(1):36-43.
【14】方建锋,田志凌,秦英,等.取向硅钢[001]晶向分布的非对称X射线衍射法测定[J].钢铁研究学报,2008,20(5):48-51.
【15】胡建民,王蕊,王春婷,等.晶体X射线衍射模型和布拉格方程的一般推导[J].大学物理,2015,34(3):1-2.
【16】李赛.超薄无取向硅钢研发[D].呼和浩特:内蒙古工业大学,2020.
【17】崔凤娥,杨平,毛卫民.取向硅钢中高斯晶粒异常长大选择性行为[J].北京科技大学学报,2010,32(9):1157-1162.
相关信息
