Creep Fracture Characteristics of Nickel-Based Single Crystal Superalloy at Different Temperatures
摘 要
在不同条件(760℃/750 MPa、850℃/500 MPa、980℃/260 MPa、1 050℃/140 MPa)下对DD407单晶高温合金进行蠕变试验,观察了蠕变断口形貌以及蠕变断裂后的显微组织和位错,分析了蠕变断裂机制。结果表明:在760℃下,试验合金发生滑移剪切断裂,γ'强化相稍有变形,但未出现明显筏排化结构;蠕变位错主要分布在γ/γ'相界面处,仅有少量位错切入γ'相。在850℃下合金仍主要发生滑移剪切断裂,γ'相开始出现筏排化;在980℃和1 050℃下,合金发生韧性断裂,并且γ'相筏排化随蠕变温度升高而越发严重;在1 050℃/140 MPa条件下γ基体通道出现大量位错塞积,大量位错以长直的位错线形态切入γ'相。
Abstract
Creep tests were carried out on DD407 single crystal superalloy under different conditions (760℃/750 MPa, 850℃/500 MPa, 980℃/260 MPa, 1 050℃/140 MPa). The creep fracture morphology and the microstructure and dislocations after creep fracture were observed. The mechanism of creep fracture was analyzed. The results show that at 760℃, the test alloy fractured in slip shear modes, and the strengthening phase γ' was slightly deformed, but no obvious rafting structures were found; creep dislocations were mainly distributed at the γ/γ' phase interface, and only a small number of dislocations entered the γ' phase. At 850℃, the alloy still mainly fractured in slip shear modes, and the γ' phase began to show rafting structures. At 980℃ and 1 050℃, the alloy had ductile fracture, and the rafting of the γ' phase became more serious with the creep temperature. Under the condition of 1 050℃/140 MPa, a large number of dislocations were packed in the γ matrix channel, and a large number of dislocations cut into the γ' phase in the form of long straight dislocation lines.
中图分类号 TG132.32 DOI 10.11973/jxgccl202210010
所属栏目 试验研究
基金项目
收稿日期 2021/5/13
修改稿日期 2022/5/22
网络出版日期
作者单位点击查看
备注韩凤奎(1977-),男,山东泰安人,高级工程师,硕士
引用该论文: HAN Fengkui,LIU Beilei,WU Baoping,XUE Xin,ZHAO Jingxuan. Creep Fracture Characteristics of Nickel-Based Single Crystal Superalloy at Different Temperatures[J]. Materials for mechancial engineering, 2022, 46(10): 56~60
韩凤奎,刘蓓蕾,吴保平,薛鑫,赵敬轩. 不同温度下镍基单晶高温合金蠕变断裂特征[J]. 机械工程材料, 2022, 46(10): 56~60
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参考文献
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【2】曹腊梅, 刘丽君, 陈晶阳, 等.热等静压温度对第三代单晶高温合金DD10组织的影响[J].材料工程, 2013, 41(6):1-4. CAO L M, LIU L J, CHEN J Y, et al.Effect of hot isostatic pressing temperature on the microstructure of a third generation single crystal superalloy DD10[J].Journal of Materials Engineering, 2013, 41(6):1-4.
【3】BOKSTEIN B S, EPISHIN A I, LINK T, et al.Model for the porosity growth in single-crystal nickel-base superalloys during homogenization[J].Scripta Materialia, 2007, 57(9):801-804.
【4】HART R V, GAYTER H.Recovery of mechanical properties in nickel alloys by re-heat-treatment[J].Journal of the Institute of Metals, 1968, 96(11):338-344.
【5】REED R C, RAE C M F. Physical metallurgy of the nickel-based superalloys[M]//Physical Metallurgy.[S.l.]:Elsevier, 2014:2215-2290.
【6】CHATTERJEE D, HAZARI N, DAS N, et al.Microstructure and creep behavior of DMS4-type nickel based superalloy single crystals with orientations near 〈001〉 and 〈011〉[J].Materials Science and Engineering:A, 2010, 528(2):604-613.
【7】ZHAO G Q, TIAN S G, ZHANG S K, et al.Deformation and damage features of a Re/Ru-containing single crystal nickel base superalloy during creep at elevated temperature[J].Progress in Natural Science:Materials International, 2019, 29(2):210-216.
【8】苏勇, 田素贵, 于慧臣, 等.镍基单晶高温合金中温稳态蠕变期间的变形机制[J].金属学报, 2015, 51(12):1472-1480. SU Y, TIAN S G, YU H C, et al.Deformation mechanisms of Ni-based single crystal superalloys during steady-state creep at intermediate temperatures[J].Acta Metallurgica Sinica, 2015, 51(12):1472-1480.
【9】BUFFIERE J Y, IGNAT M. A dislocation based criterion for the raft formation in nickel-based superalloys single crystals[J]. Acta Metallurgica et Materialia, 1995, 43(5):1791-1797.
【10】POLLOCK T M, ARGON A S. Creep resistance of CMSX-3 nickel base superalloy single crystals[J]. Acta Metallurgica et Materialia, 1992, 40(1):1-30.
【11】JACOME L A, NÖRTERSHÄUSER P, HEYER J K, et al. High-temperature and low-stress creep anisotropy of single-crystal superalloys[J]. Acta Materialia, 2013, 61(8):2926-2943.
【12】JÁCOME L A, NÖRTERSHÄUSER P, SOMSEN C, et al.On the nature of γ' phase cutting and its effect on high temperature and low stress creep anisotropy of Ni-base single crystal superalloys[J].Acta Materialia, 2014, 69:246-264.
【13】MÄLZER G, HAYES R W, MACK T, et al.Miniature specimen assessment of creep of the single-crystal superalloy LEK94 in the 1000℃ temperature range[J].Metallurgical and Materials Transactions A, 2007, 38(2):314-327.
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