Ultrasonic Nondestructive Characterization for Sensitization Degrees of 304 Stainless Steel
摘 要
将三种不同固溶状态下的304不锈钢在650 ℃下敏化处理2, 6, 16 h, 然后进行超声检测, 以探讨无损评价304不锈钢敏化程度的可行性与表征参数。结果表明: 延长敏化时间会使304不锈钢敏化程度增大; 采用衰减系数、峰值频率和峰值幅度这三个指标可以无损表征304不锈钢的敏化程度, 但声速对不同敏化处理条件下钢微观结构的改变不能够响应; 随敏化时间的延长, 钢的衰减系数会不断增大, 原因归结为敏化使得钢的晶界上出现大量铬的碳化物对超声波散射作用增强所致; 峰值频率随敏化时间的延长向高频方向偏移, 其峰值幅度也会明显上升。
Abstract
304 stainless steel samples in three different solid solution states after sensitization treatment at 650 ℃ for 2, 6 and 16 hours were evaluated employing ultrasonic testing in order to discuss the feasibility and ultrasonic nondestructive characterization parameters for the sensitization degree of 304 stainless steel. The results show that the sensitization degree of 304 stainless steel increased with prolonging the sensitization treatment time. Using attenuation coefficient, peak frequency and peak amplitude could nondestructively characterize the sensitization degree of 304 stainless steel, but ultrasonic velocity could not respond to microstructure changes under different sensitized conditions. With prolonging the sensitization treatment time, the attenuation coefficient increased gradually, which was mainly attributed to the deposition of plentiful chromium carbides along the grain boundaries, increasing the scattering of ultrasonic wave. The peak frequency exhibited a shifting to high frequency direction and the peak amplitude increased obviously with prolonging the sensitization treatment time.
中图分类号 TG115.28
所属栏目 新材料新工艺
基金项目 国家自然科学基金资助项目(51134013)
收稿日期 2012/2/21
修改稿日期 2012/10/17
网络出版日期
作者单位点击查看
备注李萍(1969-), 女, 辽宁大连人, 副教授, 博士。
引用该论文: LI Ping,CHENG Xiang-mei,LI An-na,TANG Zi-qiao. Ultrasonic Nondestructive Characterization for Sensitization Degrees of 304 Stainless Steel[J]. Materials for mechancial engineering, 2013, 37(3): 53~57
李萍,程向梅,李安娜,唐子乔. 304不锈钢敏化程度的超声无损表征[J]. 机械工程材料, 2013, 37(3): 53~57
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参考文献
【1】STELLA J, CEREZO J, RODRIGUEZ E. Characterization of the sensitization degree in the AISI 304 stainless steel using spectral analysis and conventional ultrasonic techniques[J].NDT&E International,2009, 42: 267-274.
【2】姜勇,巩建鸣,李峰. 敏化对304L不锈钢在高温NaOH溶液中应力腐蚀开裂的影响[J].机械工程材料,2010,34(2):35-38.
【3】YANLIANG H, KINSELLA B, BECKER T. Sensitization identification of stainless steel to intergranular stress corrosion cracking by atomic force microscopy[J].Mater Lett,2007,12(13):1863-1866.
【4】TAKAYA S, SUZUKI T, MATSUMOTO Y, et al. Estimation of stress corrosion cracking sensitivity of type 304 stainless steel by magnetic force microscope[J].J Nucl Mater,2004,327:19-26.
【5】BI H Y, WANG Z J, SHIMADA M, et al. Electron microscopic observation of grain boundary of thermechanical-processed SUS 304 stainless steel[J].Mater Lett,2003,57:2803-2806.
【6】杨冰,林莉,赵建强,等. 用相对衰减系数无损表征30Mn2SiV钢的显微组织[J].机械工程材料,2007,31(3):40-43.
【7】李萍,李会玲,李喜孟. 基于自回归模型参数超声无损评价20钢的时效组织[J].机械工程材料,2006,30(8):25-27.
【8】《超声波探伤技术及探伤仪》编写组.超声波探伤技术及探伤仪[M].北京:国防工业出版社,1977:14-15.
【9】田莳. 材料物理性能[M].北京:北京航空航天大学出版社,2004:81-392.
【10】李夫舍茨.金属与合金的物理性能[M].王润,译.北京:机械工业出版社,1961:215-216.
【11】张颜艳.奥氏体不锈钢组织超声无损评价研究[D].南昌: 南昌航空大学,2010.
【12】ADLER L, WHALEY H L. Interference effect in a multifrequency ultrasonic pulse echo and its application to flaw characterization[J].J Acoust Soc Am,1971,51(3):881-887.
【2】姜勇,巩建鸣,李峰. 敏化对304L不锈钢在高温NaOH溶液中应力腐蚀开裂的影响[J].机械工程材料,2010,34(2):35-38.
【3】YANLIANG H, KINSELLA B, BECKER T. Sensitization identification of stainless steel to intergranular stress corrosion cracking by atomic force microscopy[J].Mater Lett,2007,12(13):1863-1866.
【4】TAKAYA S, SUZUKI T, MATSUMOTO Y, et al. Estimation of stress corrosion cracking sensitivity of type 304 stainless steel by magnetic force microscope[J].J Nucl Mater,2004,327:19-26.
【5】BI H Y, WANG Z J, SHIMADA M, et al. Electron microscopic observation of grain boundary of thermechanical-processed SUS 304 stainless steel[J].Mater Lett,2003,57:2803-2806.
【6】杨冰,林莉,赵建强,等. 用相对衰减系数无损表征30Mn2SiV钢的显微组织[J].机械工程材料,2007,31(3):40-43.
【7】李萍,李会玲,李喜孟. 基于自回归模型参数超声无损评价20钢的时效组织[J].机械工程材料,2006,30(8):25-27.
【8】《超声波探伤技术及探伤仪》编写组.超声波探伤技术及探伤仪[M].北京:国防工业出版社,1977:14-15.
【9】田莳. 材料物理性能[M].北京:北京航空航天大学出版社,2004:81-392.
【10】李夫舍茨.金属与合金的物理性能[M].王润,译.北京:机械工业出版社,1961:215-216.
【11】张颜艳.奥氏体不锈钢组织超声无损评价研究[D].南昌: 南昌航空大学,2010.
【12】ADLER L, WHALEY H L. Interference effect in a multifrequency ultrasonic pulse echo and its application to flaw characterization[J].J Acoust Soc Am,1971,51(3):881-887.
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