Quantitative Analysis of Kyanite Sample with X-ray Diffractometry
摘 要
提出了应用X射线衍射法定量分析蓝晶石样品。将粒径10~15 μm的蓝晶石粉末置于模具中,制成厚度为0.2 mm的样片。取经提纯的蓝晶石和纯石英,按不同比例配成11个校准样品用于制作工作曲线,每一样品中加入相同量的刚玉作为内标以校正基体干扰。方法用于蓝晶石地质样品分析,所得测定结果与理论值相符。
Abstract
A method of X-ray diffraction (XRD) for quantitative analysis of kyanite was proposed. The sample was powdered to size between 10 and 15 μm, and pressed in a mould to form a sample wafer with its thickness of 0.2 mm. Eleven calibration samples were prepared by mixing purified kyanite and pure quartz in various proportions and were used for preparation of working curve; same amounts of corundum were added separately to each sample as internal standard for correction of matrix interference. The proposed method was used in the analysis of geological sample of kyanite, and the results obtained were checked quite well with the theoratical values.
中图分类号 O657.34
所属栏目 工作简报
基金项目 国土资源部公益性行业科研专项资助(200911043-06)
收稿日期 2012/10/18
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备注杜晓冉(1973-),女,河南洛阳人,工程师,主要从事岩矿鉴定工作。
引用该论文: DU Xiao-ran,ZHI Hong-mei,ZHANG Jin-kuang,ZHOU Jiao-hua,WANG Juan,CHEN Jing,CHEN Jin-shen. Quantitative Analysis of Kyanite Sample with X-ray Diffractometry[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2013, 49(4): 402~404
杜晓冉,智红梅,张金矿,周姣花,王娟,陈静,陈金身. X射线衍射法定量分析蓝晶石样品[J]. 理化检验-化学分册, 2013, 49(4): 402~404
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参考文献
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【2】刘仕子.X射线衍射定量相分析的策略架构[J].岩矿测试, 2001,20(2):81-87.
【3】马礼敦.近代X射线多晶体衍射[M].北京:化学工业出片社, 2004:482-484.
【4】郭常霖.求解X射线定量分析最小二乘方程组的抛弃平均法[J].金属学报, 1991,49(3):202-206.
【5】马礼敦.X射线粉末衍射的新起点——Rietveld[M].北京:化学工业出片社, 2004:482-484.
【6】刘粤惠,刘平安.X射线衍射分析原理与应用[M].北京:化学工业出版社, 2003:72-77.
【7】迟广成,张泉,赵爱林.X射线粉晶衍射仪定量测量海泡石矿样的实验条件[J].岩矿测试, 2012,31(2):282-286.
【8】吴建鹏,黄剑峰,贺海燕,等.X射线衍射物相定量分析内标法标准曲线库的建立[J].岩矿测试, 2006,25(3):215-218.
【9】叶大年.X射线粉末法及其在岩石学中的应用[M].北京:科学出版社, 1984:76-128.
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