GC DETERMINATION OF RESIDUAL BENZENE HOMOLOGUES IN CIGARETTE PACKAGING PAPERBOARD BY SAMPLING WITH PURGETRAPPING METHOD
摘 要
采用吹扫捕集气相色谱法测定卷烟包装卡纸中苯系物残留,并对测试条件进行了优化.所测定的苯、甲苯、乙苯、对二甲苯、间二甲苯、邻二甲苯、苯乙烯等在4.3-900 μg·L-1浓度范围具有良好的线性,相关系数均达到0.999 9,检出限为1.0-11.6 ng·g-1,回收率为91.5%-1092%,重复测定5次的相对标准偏差为1.73%-3.24%.
Abstract
The purge-trapping method was applied to the sampling in GC determination of residual benzene homologues in cigarette packing paperboard.Linear relationships between peak area and concentration of benzene homologue were obtained in the range of 4.3-900 μg·L-1 for all of the 6 homologues tested (i.e.benzene,toluene,ethyl benzene,m-xylene,o-xylene,m-xylene and styrene) with their correlation coefficients achieved to 0.999 9.Detection limits were ranged between 1.0 to 11.6 ng·g-1.Recoveries obtained were in the range of 91.5%-109.2%.RSD′s (n=5) found were in the range of 1.73%-3.24% for the 6 homologues.
中图分类号 O657.37
所属栏目 试验与研究
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收稿日期 2005/11/2
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备注冯建跃(1960-),男,浙江杭州人,教授,主要从事色谱理论与技术研究.
引用该论文: KE Ying-fen,FENG Jian-yue,CHEN Guan-xi,ZHAO Yong-xin. GC DETERMINATION OF RESIDUAL BENZENE HOMOLOGUES IN CIGARETTE PACKAGING PAPERBOARD BY SAMPLING WITH PURGETRAPPING METHOD[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2006, 42(7): 509~510
柯颖芬,冯建跃,陈关喜,赵永信. 吹扫捕集气相色谱法测定卷烟包装卡纸中苯系物残留[J]. 理化检验-化学分册, 2006, 42(7): 509~510
被引情况:
【1】李永亮,李健,李桂莲,于亭亭, "吹扫捕集-气相色谱法测定水稻田土壤中的敌稗",理化检验-化学分册 52, 1073-1075(2016)
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【3】周密,刘德全,林旭,等.吹扫捕集/气相色谱法测定空气中挥发性有机物[J].中国环境监测,2004,20(4):12.
【4】陈珠灵,张兰,吴晓苹,等.固相微萃取-气相色谱技术用于涂料中苯系物有害物质的快速测定[J].福州大学学报:自然科学版,2004,32(6):751.
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