A Modified FI-Differential Spectrophotometric Method for Determination of Total Saccharides in Pumpkin
摘 要
采用自行研制的两组流动比色装置,分别安装在检测器的样品光束和参比光束位置,提出了一种改进的流动注射微分分光光度测定南瓜提取物总糖含量的方法.一次进样同时产生6个拐点的微分吸收曲线(A1、A2、A3、A4、A5、A6).根据各拐点所测得的响应信号值,求得糖的质量浓度在0.3~46 mg·L-1范围内呈线性关系.为检测方法的精密度和回收率分析了3个已知样品并加入11 mg·L-1糖标准溶液,测得方法的相对标准偏差(n=5)在0.6%~1.3%之间,回收率在98.7%~101.2%之间.
Abstract
Manifold of a FI-spectrophotometric installation for determination of total saccharides in pumpkin was designed and fabricated.Two sets of self-made flow-cells were installed separately in the light paths of sample and blank (or reference) solution.As shown in the figure,6 inflection points (A1,A2,A3,A4,A5 and A6) were observed in the differential absorption curve at one sample introduction.Based on the response signals at the inflection points,linear relationships between values of ΔAT and concentration of total saccharides was obtained in the range of 0.3-46 mg·L-1.Tests for precision and recovery were made on analysis of 3 samples of known contents of total saccharides and of addition of 11 mg·L-1 of standard saccharide solutions,values of RSD′s (n=5) found were ranged from 0.6% to 1.3%,and values of recovery in the range of 98.7%-101.2% were obtained.
中图分类号 O657.32
所属栏目 工作简报
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收稿日期 2008/11/17
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备注赵珍义(1952-),男,大连市人,副教授,研究方向为天然药物的合成及动态在线检测分析.
引用该论文: ZHAO Zhen-yi,SONG Jin-he,YU Ji,LI Kun,YU He. A Modified FI-Differential Spectrophotometric Method for Determination of Total Saccharides in Pumpkin[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2009, 45(11): 1305~1307
赵珍义,宋金和,于吉,李鲲,于合. 一种改进的流动注射微分分光光度法测定南瓜总糖含量[J]. 理化检验-化学分册, 2009, 45(11): 1305~1307
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参考文献
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【2】彭红,黄小莉,欧阳友生,等.南瓜多糖的提取工艺及其降糖作用的研究[J].食品科学,2002,23(8):261-263.
【3】名和能治.南瓜粉对轻度糖尿病患者有惊人的效果[J].大众医学,1982(9):31-32.
【4】刘宜生.南瓜的开发与利用[J].中国食物与营养,2001(5):19-23.
【5】耿越,赵相轩,花义山,等.高效毛细管电泳法测定蜂蜜中单糖的含量[J].食品科学,2002,23(1):114-116.
【6】杨文菊,田树革,董文杰,等.紫外光谱法测定蜂蜜中总糖含量[J].光谱实验室,2007,24(4):739-742.
【7】赵珍义.沉积物中铝含量的流动注射分光光度法测定[J].分析化学,1996,24(4):456-458.
【8】赵珍义,韩光喜,赵晔,等.FIA微分光度法测定合金钢中钒的含量[J].光谱实验室,2007,24(4):256-268.
【9】赵珍义.多孔流动注射比色装置:912110726[P].1992-05-20.
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