Microstructure and Magnetic Properties of Strip-Casting Non-oriented Silicon Steel at Different Cold Rolling and Annealing Processes
摘 要
针对1.5 mm厚双辊薄带连铸Fe-1.3%Si无取向硅钢铸带在不同变形量(56.7%, 66.7%, 76.7%)下进行冷轧, 之后再在不同温度(800, 850, 900, 950 ℃)和时间(1, 3, 5, 7 min)下进行退火处理, 研究了硅钢的显微组织、析出相和磁性能。结果表明: 在退火过程中钢中的析出物以MnS为主, 其尺寸主要在30~40 nm之间, 对晶粒的钉扎作用较为明显; 退火硅钢的磁感B50稳定在1.77~1.80 T; 随着变形量从56.7%增大到76.7%, 再结晶晶粒明显细化, 退火硅钢的铁损P15/50从5.54 W·kg-1下降到4.23 W·kg-1; 变形量为66.7%的硅钢在900 ℃退火5 min后, 再结晶晶粒较大, 硅钢的磁性能最优, P15/50约为4.54 W·kg-1。
Abstract
A 1.5 mm thickness Fe-1.3%Si non-oriented silicon steel as-cast strip produced by strip casting was cold rolled at different reductions (56.7%, 66.7%, 76.7%) and annealed at different temperatures (800, 850, 900, 950 ℃) and time (1, 3, 5, 7 min). The microstructure, precipitate and magnetic properties of the silicon steel were investigated. The results show that MnS particles with size of 30-40 nm were the main precipitate during annealing, which had significantly pinning effect on grain. The magnetic induction B50 of annealed silicon steel maintained at 1.77-1.80 T. With the increase of cold rolling reduction from 56.7% to 76.7%, the average size of recrystallized grains refined obviously and core loss P15/50 decreased from 5.54 W·kg-1 to 4.23 W·kg-1. Relatively large recrystallized grains were obtained when the cold rolled silicon steel with 66.7% reduction was annealed at 900 ℃ for 5 min, leading to the optimal magnetic properties (P15/50= 4.54 W·kg-1).
中图分类号 TG142.1 TG156.2 DOI 10.11973/jxgccl201605004
所属栏目 试验研究
基金项目 国家自然科学基金资助项目(51174059, 51404155, U1260204); 中央高校基本科研业务费资助项目(N130407003); 新世纪优秀人才支持计划资助项目(NCET-13-0111); 辽宁省高等学校优秀人才支持计划资助项目(LR2014007)
收稿日期 2015/4/7
修改稿日期 2016/3/10
网络出版日期
作者单位点击查看
备注谢顺卿(1992-), 男, 安徽淮北人, 硕士研究生。
引用该论文: XIE Shun-qing,JIAO Hai-tao,HAN Qiong-qiong,ZHANG Yuan-xiang,WANG Yang,CAO Guang-ming,LI Cheng-gang,XU Yun-bo. Microstructure and Magnetic Properties of Strip-Casting Non-oriented Silicon Steel at Different Cold Rolling and Annealing Processes[J]. Materials for mechancial engineering, 2016, 40(5): 25~30
谢顺卿,焦海涛,韩琼琼,张元祥,王洋,曹光明,李成刚,许云波. 不同冷轧退火工艺下薄带连铸无取向硅钢的组织和磁性能[J]. 机械工程材料, 2016, 40(5): 25~30
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【4】董廷亮, 岳尔斌, 李建军, 等. 常化温度对 TSCR 流程制备低碳低硅无取向硅钢组织和性能的影响[J]. 机械工程材料, 2011, 35(3): 15-17.
【5】GE S, ISAC M, GUTHRIE R I L. Progress of strip casting technology for steel: historical developments [J]. ISIJ International, 2012, 52(12): 2109-2122.
【6】LIU Z Y, LIN Z S, QIU Y Q, et al. Segregation in twin roll strip cast steels and the effect on mechanical properties [J]. ISIJ International, 2007, 47(2): 254-258.
【7】WANG L T, DENG C H, DONG M, et al. Development of continuous casting technology of electrical steel and new products [J]. Journal of Iron and Steel Research, International, 2012, 19(2): 1-6.
【8】ZHANG Y X, XU Y B, LIU H T, et al. Microstructure, texture and magnetic properties of strip-cast 1.3%Si non-oriented electrical steels [J]. Journal of Magnetism and Magnetic Materials, 2012, 324(20): 3328-3333.
【9】LIU H T, LIU Z Y, LI C G, et al. Solidification structure and crystallographic texture of strip casting 3wt%Si non-oriented silicon steel[J]. Materials Characterization, 2011, 62(5): 463-468.
【10】朱涛, 裴英豪, 李昌义, 等. CSP生产无取向电工钢的组织和性能[J]. 钢铁, 2009, 44(3): 67-70.
【11】马良, 项利, 仇圣桃, 等. 双辊薄带连铸3.98%Si-0.71%Al无取向硅钢的组织、织构和磁性能[J]. 机械工程材料, 2014, 38(1): 47-51.
【12】雍歧龙. 钢铁材料中的第二相[M]. 北京: 冶金工业出版社, 2006.
【13】XU Y B, ZHANG Y X, WANG Y, et al. Evolution of cube texture in strip-cast non-oriented silicon steels [J]. Scripta Materialia, 2014, 87: 17-20.
【14】何忠治, 赵宇, 罗海文. 电工钢[M]. 北京: 冶金工业出版社, 2012.
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