Preparation of Metallographic Specimens of Low Alloy Steel Welding Joints for Macroscopic Inspection
摘 要
某出口低合金钢转向架焊接构架的焊接工艺评定对该焊接接头的低倍检验有较高的要求。通过合理配制腐蚀溶液, 增加腐蚀溶液的种类, 并严格规范腐蚀步骤, 确定了合理的低倍检验用金相试样的制备工艺。结果表明: 使用8%硝酸酒精溶液(体积分数)及过硫酸铵饱和水溶液制备的焊接接头金相试样各区域清晰可见, 制样质量稳定, 能够满足该焊接构架的焊接工艺评定要求。
Abstract
According to qualification requirements of the welding procedure of the exported welding bogie frame made from low alloy steel, the requirement of the macroscopic inspection of the welding joints was relatively high. Through reasonably preparing the corrosive solution, increasing the type of corrosion solution, and strictly regulating the corrosion process, the reasonable preparation process of metallographic specimens for macroscopic inspection was determined. The results show that: each region of the metallographic specimens of the welding joints corroded by 8% (volume fraction) nitric acid alcohol solution and saturated aqueous solution of ammonium peroxydisulfate was distinct, and the preparation quality was stable, which could fully meet qualification requirements of the welding procedure.
中图分类号 TG115.21 DOI 10.11973/lhjy-wl201611009
所属栏目 试验技术与方法
基金项目
收稿日期 2016/3/25
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备注杨黎明(1985-), 男, 工程师, 学士, 主要从事理化检测工艺方面的研究,
引用该论文: YANG Li-ming,DAN Chu-chen. Preparation of Metallographic Specimens of Low Alloy Steel Welding Joints for Macroscopic Inspection[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2016, 52(11): 790~792
杨黎明,但楚臣. 低合金钢焊接接头低倍检验金相试样的制备[J]. 理化检验-物理分册, 2016, 52(11): 790~792
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参考文献
【1】BS EN 1321-1997 金属材料焊缝的破坏试验 焊缝宏观和微观检验[S].
【2】ISO 15614.1-2004 金属材料焊接程序的规范和鉴定[S].
【3】ISO 5817-2014 焊接——钢、镍、钛及其合金的熔焊接缝(不含电子束焊)——缺陷质量分类[S].
【4】ISO/TR 16060-2003 金属材料的破坏性试验——宏观和微观检验用腐蚀剂[S].
【5】桂立丰,唐汝钧.机械工程材料测试手册:物理金相卷[M].沈阳:辽宁科学技术出版社,1999:10.
【2】ISO 15614.1-2004 金属材料焊接程序的规范和鉴定[S].
【3】ISO 5817-2014 焊接——钢、镍、钛及其合金的熔焊接缝(不含电子束焊)——缺陷质量分类[S].
【4】ISO/TR 16060-2003 金属材料的破坏性试验——宏观和微观检验用腐蚀剂[S].
【5】桂立丰,唐汝钧.机械工程材料测试手册:物理金相卷[M].沈阳:辽宁科学技术出版社,1999:10.
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