Microstructure and Properties of SiCp/Al Composite Prepared by Powder Extrusion Forming
摘 要
采用粉末挤压成型方法制备SiC体积分数分别为30%,40%,50%的SiCp/Al复合材料,通过光学显微镜、扫描电镜、拉伸试验机、布氏硬度计、热膨胀仪和热导率测试仪等对其显微组织、力学性能和物理性能等进行了分析。结果表明:经过450℃热挤压成型成功制备出30% SiCp/Al和40% SiCp/Al复合材料,而50% SiCp/Al复合材料无法直接挤压成型;在复合材料纵截面上,铝基体沿挤压方向分布并呈现白色条状流线型组织;两种复合材料的拉伸断口均由大量细小韧窝组成,呈混合断裂特征;随着SiC体积分数的提高,复合材料布氏硬度从81.9 HB升高到98 HB,但抗拉强度有所降低,伸长率明显减小;复合材料的相对密度和线膨胀系数减小,热导率增大。
Abstract
The SiCp/Al composites with SiC volume fraction of 30%, 40% and 50% were prepared by powder extrusion forming. The microstructure, mechanical properties and physical properties of different SiCp/Al composites were analyzed by optical microscopy, scanning electron microscopy, tensile tester, brinell hardness tester, thermodilatometer and thermal conductivity detector. The results showed that 30% and 40% SiCp/Al composites could be extruded in 450℃, but 50% SiCp/Al composite failed. On longitudinal section of composite, the aluminum matrix was distributed along the extrusion direction and presented the white strip streamline structure. The tensile fracture surface of two composites was made up of a large number of smaller dimples, both of which presented mixed fracture characteristics. With increase of SiCp volume fraction, the brinell hardness increased from 81.9 HB to 98 HB while tensile strength decreased slightly and the elongation reduced obviously. The relative density and coefficient of linear expansion of the composite reduced while thermal conductivity improved.
中图分类号 TB333 DOI 10.11973/jxgccl201707009
所属栏目 试验研究
基金项目 湖南省战略性新兴产业科技攻关与重大科技成果转化项目(2014GK1063)
收稿日期 2016/6/6
修改稿日期 2017/5/25
网络出版日期
作者单位点击查看
备注蔡翔(1991-),男,湖南长沙人,硕士研究生
引用该论文: CAI Xiang,ZHANG Hui,CHEN Shuang. Microstructure and Properties of SiCp/Al Composite Prepared by Powder Extrusion Forming[J]. Materials for mechancial engineering, 2017, 41(7): 43~48
蔡翔,张辉,陈爽. 粉末挤压成型制备SiCp/Al复合材料的显微组织及性能[J]. 机械工程材料, 2017, 41(7): 43~48
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【4】LATIEF F H, SHERIF E S M. Effects of sintering temperature and graphite addition on the mechanical properties of aluminum[J]. Journal of Industrial and Engineering Chemistry, 2012, 18(6):2129-2134.
【5】高增,王西涛,牛济泰,等.表面镀镍SiCp/Al复合材料与可伐合金的真空钎焊[J]. 机械工程材料,2014,38(12):20-24.
【6】武高辉,姜龙涛,修子扬,等.仪表级SiC/Al复合材料的应用研究与实践[J]. 导航与控制,2010,9(1):66-70.
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【8】EUH K, KANG S B, YANG B M, et al. Effect of process parameters on the fabrication of Al-SiC composite sheets by atmospheric plasma spraying method[J]. Journal of the Korean Institute of Metals and Materials,2003,41(6):342-350.
【9】XU Y, TANAKA Y, GOTO M, et al. Thermal conductivity of SiC fine particles reinforced Al alloy matrix composite with dispersed particle size[J]. Journal of Applied Physics, 2004, 95(2):722-726.
【10】石锋,钱瑞芬,张志萍,等. SiCp/Al复合材料的应用及无压渗透法制备[J]. 硅酸盐通报,2004,23(2):60-66.
【11】韩桂泉. 高体分SiCp/Al复合材料新型制备工艺研究[J]. 陶瓷,2005(6):22-24.
【12】张颖骁. 高含量SiC颗粒增强铝基复合材料制备及性能研究[D]. 北京:北京交通大学,2015.
【13】郝世明. 中体积分数SiCp/Al复合材料的制备和微结构及性能研究[D]. 郑州:郑州大学,2015.
【14】侯德宝. 粉末挤压法制备SiC颗粒增强镁基复合材料的研究[D]. 沈阳:东北大学,2008.
【15】GAIN A K, HAN J K, JANG H D, et al. Fabrication of continuously porous SiC-Si3N4 composite using SiC powder by extrusion process[J]. Journal of the European Ceramic Society, 2006, 26(13):2467-2473.
【16】沈茹娟,孙超,宋旼,等.混料时间和挤压对SiC增强纯Al基复合材料显微组织和力学性能的影响[J]. 粉末冶金材料科学与工程,2012,17(5):604-610.
【17】张大童,李元元,罗宗强,等.快速凝固高硅铝合金粉末的热挤压过程[J]. 中国有色金属学报,2001,11(1):6-9.
【18】SHARMA S C. Effect of particles on the coefficient of thermal expansion behavior of the A16061 alloy composites[J]. Metallurgical and Materials Transactions A, 2000, 31(3):773-780.
【19】熊兆贤. 材料物理导论[M].北京:科学出版社,2001:59-65.
【20】郝亮.喷射沉积SiCp/FVS1012及SiCp/FVS1212复合材料后续加工及组织性能的研究[D].长沙:湖南大学,2008.
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