0.100 0 g核级海绵锆样品用氢氟酸0.5 mL，硝酸2 mL于150℃左右溶解后，用水定容至100 mL。采用电感耦合等离子体质谱法测定样品溶液中钨的含量。¹⁸⁴W为分析核素，以²³²Th为内标物。钨的线性范围在100.0 μg·L^-1以内，方法的检出限（3s）为0.003 μg·L^-1。以2.00，50.00 μg·L^-1浓度水平进行加标回收试验，回收率为91.5%，93.5%，测定值的相对标准偏差（n=6）为5.0%，2.4%。

The sample (0.100 0 g) of nuclear grade sponge zirconium was dissolved with HF (0.5 mL) and HNO₃ (2 mL) at temperature of 150℃ or so,and then was diluted to 100 mL with water. ICP-MS was applied to the determination of W in the sample solution. ¹⁸⁴W was used as the analytical nuclide, ²³²Th was used as internal standard. Linearity range of W was found in the range within 100.0 μg·L^-1 with detection limit (3s) of 0.003 μg·L^-1. Tests for recovery was made by standard addition method at the concentration levels of 2.00, 50.00 μg·L^-1, values of recovery found were 91.5%,93.5%, with RSD's (n=6) of 5.0%, 2.4%.