Determination of Phase Transformation Temperatures of Zr-Sn and Zr-Nb Zircaloys by Metallographic Method
摘 要
采用金相法测定了锆锡系Zr4锆合金和锆铌系N36锆合金由α+β相转变为β相的相变温度Tα+β→β。结果表明:可以通过金相法测定锆合金的相变温度Tα+β→β,在相变温度Tα+β→β附近淬火,通过观察试样α相含量的变化,确定α相未完全转变和完全转变的温度区间,相变温度Tα+β→β取该区间的下限值,热处理加热温度间隔建议选择为10℃;试验测得Zr4锆合金的Tα+β→β为970℃,N36锆合金的Tα+β→β为890℃。
Abstract
The phase transformation temperature Tα+β→β from α + β phase to β phase of Zr-4 and N36 zircaloys was determined by metallographic method. The results show that the phase transformation temperature Tα+β→β of zircaloys could be determined by metallographic method. By quenching the samples at the temperatures near the phase transformation temperature Tα+β→β and then observing the change of α phase contents, the temperature range of incomplete transformation and complete transformation of α phase was determined, and the lower limit value of the temperature range was taken as the phase transformation temperature Tα+β→β. The recommended heat treatment heating temperature interval was 10℃. The measured Tα+β→β of Zr-4 zircaloy was 970℃, and the Tα+β→β of N36 zircaloy was 890℃.
中图分类号 TG146.4 DOI 10.11973/lhjy-wl201802007
所属栏目 试验技术与方法
基金项目
收稿日期 2017/3/13
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备注马红征(1969-),女,教授级高工,主要从事稀有金属的组织分析及研究,baojimhz@163.com
引用该论文: MA Hongzheng,ZHAI Tongde,SHI Kexue,ZHANG Jing,SUN Xiaofeng,HOU Xiaoyu,WANG Feng,WANG Shaofeng,HE Wei. Determination of Phase Transformation Temperatures of Zr-Sn and Zr-Nb Zircaloys by Metallographic Method[J]. Physical Testing and Chemical Analysis part A:Physical Testing, 2018, 54(2): 115~118
马红征,翟通德,石科学,张靖,孙晓峰,侯小宇,王峰,王少峰,何伟. 金相法测定锆锡和锆铌系锆合金的相变温度[J]. 理化检验-物理分册, 2018, 54(2): 115~118
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参考文献
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【2】梁建烈,庄应烘,赵文金,等. 新锆合金的相变温度[J]. 广西科学,2002,9(3):181-185.
【3】唐普放. 钛及钛合金相变温度与测定[J]. 钛工业进展,1999,16(3):34-37.
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