超级13Cr油管在不同完井液中的应力腐蚀开裂敏感性
Stress Corrosion Cracking Sensitivity of Super 13Cr Tubing in Different Completion Fluid Environments
摘 要
通过慢应变速率试验（SSRT），结合能谱分析（EDS）和扫描电子显微镜（SEM）观察等手段，研究了超级13Cr不锈钢油管在三种油田常用磷酸盐完井液中的应力腐蚀开裂（SCC）敏感性。结果表明：超级13Cr不锈钢油管在120℃、三种磷酸盐完井液环境中均存在一定程度的SCC敏感性，且其在三种磷酸盐完井液中的腐蚀程度由弱到强依次为1号磷酸盐完井液 < 2号磷酸盐完井液 < 3号磷酸盐完井液。材料SCC敏感性的增加源于材料腐蚀的加剧和断裂韧性的下降。
磷酸盐完井液
应力腐蚀开裂
super 13Cr stainless steel
phosphate completion fluid
stress corrosion cracking
Abstract
Slow strain rate test (SSRT) combined with energy dispersive spectroscopy (EDS) and scanning electron microscopy (SEM) observations were used to study the stress corrosion cracking (SCC) susceptibility of super 13Cr stainless steel tubing in three different phosphate well completion fluids commonly used in the field. The results show that the SCC sensitivity of the super 13Cr stainless steel tubing existed in all three phosphate completion fluid environments at 120℃. And the degrees of corrosion in the three phosphate completion fluids from weak to strong were as follows:No. 1 phosphate completion fluid < No. 2 phosphate completion fluid < No. 3 phosphate completion fluid. The increase in the SCC sensitivity of the material was due to the damage of corrosion and the decline of fracture toughness.
中图分类号 TG174 DOI 10.11973/fsyfh-201807013
所属栏目 应用技术
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收稿日期 2017/3/22
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引用该论文: CHANG Zeliang,YUE Xiaoqi,LI Yan,ZHANG Lei,GENG Hailong,LU Minxu. Stress Corrosion Cracking Sensitivity of Super 13Cr Tubing in Different Completion Fluid Environments[J]. Corrosion & Protection, 2018, 39(7): 549
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参考文献
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【3】邹炯强. 宝山钢铁股份有限公司顺利完成首批BT-S13Cr110超级13Cr油管生产[J]. 钢管,2010,39(1):52-52.
【4】吕拴录,杨向同,宋文文,等. 某井超级13Cr钢特殊螺纹接头油管接箍横向开裂原因分析[J]. 理化检验(物理分册),2015,51(4):297-301.
【5】丁毅,历建爱,张国正,等. 110钢级φ88.9 mm×6.45 mm超级13Cr钢油管刺穿失效分析[J]. 理化检验(物理分册),2011,47(10):663-667.
【6】辛海鹏,王建瑶,周芝琴,等. 磷酸盐水泥固井技术在LKQ地区X井火烧油层的应用[J]. 钻井液与完井液,2016,33(3):73-83.
【7】王鹏,王新虎,韩礼红,等. 高温高压井油管完井液导致应力腐蚀开裂分析[C]//全国失效分析学术会议.[出版地不详]:[出版者不详],2015.
【8】万里平,孟英峰,卢清兰,等. 塔里木油田有机盐完井液腐蚀研究[J]. 西南石油大学学报(自然科学版),2009,31(1):133-136.
【9】万里平,孟英峰,尹成先,等. P110钢在有机盐完井液中的腐蚀行为[J]. 钻井液与完井液,2007,24(1):17-19.
【10】PENG G S,CHEN K H,CHEN S Y,et al. Effect of the deformation on the stress-corrosion cracking of Al-Zn-Mg-Cu alloys[J]. Materials & Corrosion,2012,63(63):254-258.
【11】QIAO Y X,ZHENG Y G,OKAFOR P C,et al. Electrochemical behaviour of high nitrogen bearing stainless steel in acidic chloride solution:effects of oxygen, acid concentration and surface roughness[J]. Electrochemical Acta,2009,54(8):2298-2304.
【12】TURNBULL A,GRIFFITHS A. Corrosion and cracking of weldable 13 wt% Cr martensitic stainless steels for application in the oil and gas industry[J]. Corrosion Engineering Science & Technology the International Journal of Corrosion Processes & Corrosion Control,2013,38(1):21-50.
【13】KANE R D,WILHELM S M. Status of standardization activities on slow strain rate testing techniques[J]. Research and Engineering Applications,1993(6):40-47.
【14】AHLUWALIA H S. Problems associated with slow strain rate quality assurance testing of nickel-base corrosion resistant alloy tubular in hydrogen sulfide environment[J]. Research and Engineering Applications,1993(6):225-239.
【15】WILHEIM S M,CURRIE D M. Relationship of localized corrosion and SCC in oil and gas production environments[J]. Research and Engineering Applications,1993(6):263-289.
【16】HIBNER E L. Improved SSR test for lot acceptance criterion[J]. Research and Engineering Applications,1993(6):290-294.
【17】李岩,方可伟,刘飞华. Cl-对304L不锈钢从点蚀到应力腐蚀转变行为的影响[J]. 腐蚀与防护,2012,33(11):955-959.
【18】UEMATSU Y,TOKAJI K,OHASHI T,et al. Effect of anodic oxide film on fatigue behaviour of magnesium alloys in laboratory air and demineralized water[J]. Nihon Kikai Gakkai Ronbunshu A Hen/transactions of the Japan Society of Mechanical Engineers Part A,2008,74(737):122-127.
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【21】YAO X,XIE F,XIANGQING W U,et al. Effects of Cl- concentration on stress corrosion cracking behaviors of super 13Cr tubing steels[J]. Materials Review,2012,26:33-38.
【22】GAO B,KE W. In-situ TEM observation of dissolution-enhanced dislocation emission, motion and the nucleation of SCC for Ti-24Al-11Nb alloy in methanol[J]. Scripta Materialia,1997,36(2):259-264.
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