Determination of Calcium Carbonate in Cigarette Paper and Reclaimed Tobacco Leaves Made by the Paper-Making Process by Continuous Flow Method
摘 要
取卷烟纸或造纸法再造烟叶细条(约0.5 cm×2.5 cm)样品0.500 g,与0.5 mol·L-1盐酸溶液4.5 mL反应完全,加入95.5 mL水,混匀后过滤,于滤液中加入5 g活性碳,振荡30 min,过滤,收集滤液。采用连续流动法通过碘酸钾、碘化钾与样品溶液中剩余H+的显色反应来计算剩余H+的含量,从而推算样品中碳酸钙的含量。结果表明:①碳酸钙的线性范围为5.007~30.042 mg;②方法的检出限(3s)为0.11 mg;③连续测定6次所得结果的相对标准偏差为0.34%~0.86%;④加标回收率为96.6%~103%。方法的测定值和电位滴定法的测定值基本相符,但与离子色谱法所测结果之间有一定差异。
Abstract
The sample (0.500 g) of strips (about 0.5 cm×2.5 cm) of cigarette paper or reclaimed tobacco leaves made by the paper-making process was taken and reacted completely with 4.5 mL of 0.5 mol·L-1 HCl solution. Water (95.5 mL) was added, and the mixture was mixed well and filtered. Granulated active carbon (5 g) was added to the filtrate, and the mixture was mixed thoroughly for 30 min and filtered again. The filtrate was collected and its content of calcium carbonate was determined by continuous flow method through the color reaction among KIO3, KI and H+ remained in the sample solution, and based on the content of H+ found, calcium carbonate was calculated. It was found that:① linearity range of calcium carbonate was 5.007-30.042 mg; ② detection limit (3s) of the method was 0.11 mg; ③ RSDs (n=6) for the results were found between 0.34% and 0.86%; ④ values of recovery found by standard addition method ranged from 96.6% to 103%. The results found by the present method were as a whole in consistency with those found by potentiometric titration, but obvious deviations were found as compared with the results given by ion chromatography.
中图分类号 O657 DOI 10.11973/lhjy-hx201808013
所属栏目 工作简报
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收稿日期 2017/8/20
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备注彭丽娟,高级工程师,硕士研究生,主要从事烟草、烟草制品、卷烟及其相关原辅材料的分析及研究工作,849164145@qq.com
引用该论文: PENG Lijuan,ZHANG Wei,SI Xiaoxi,WANG Chunqiong,QIAN Guangxue,NI Jun,LI Ling,CHEN Maojian,WANG Shuhua. Determination of Calcium Carbonate in Cigarette Paper and Reclaimed Tobacco Leaves Made by the Paper-Making Process by Continuous Flow Method[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2018, 54(8): 932~937
彭丽娟,张威,司晓喜,王春琼,钱光学,倪军,李苓,陈茂建,王淑华. 连续流动法测定卷烟纸和造纸法再造烟叶中碳酸钙含量[J]. 理化检验-化学分册, 2018, 54(8): 932~937
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【5】周明松,孙章建,周莉莉,等.卷烟纸中CaCO3的定量方法比较及形貌表征研究[J].分析测试学报, 2012,31(2):200-205.
【6】YC/T 314-2009卷烟纸中碳酸钙的测定电位滴定法[S].
【7】彭丽娟,李苓,张燕,等.一种测定卷烟纸中碳酸钙含量的方法:102507483B[P]. 2013-04-10.
【8】王莉,王驰,宁敏,等.国产和进口造纸法再造烟叶中无机添加物分析研究[J].中华纸业, 2015,36(24):17-21.
【9】YC/T 159-2002烟草及烟草制品水溶性糖的测定连续流动法[S].
【10】YC/T 468-2013烟草及烟草制品总植物碱的测定连续流动法[S].
【11】YC/T 161-2002烟草及烟草制品总氮的测定连续流动法[S].
【12】YC/T 162-2002烟草及烟草制品氯的测定连续流动法[S].
【13】YC/T 245-2008烟草及烟草制品氨的测定连续流动法[S].
【14】YC/T 253-2008卷烟主流烟气中氰化氢的测定连续流动法[S].
【15】孔浩辉,程志颖,郭璇华,等.烟草中果胶含量连续流动测定方法的改进[J].烟草科技, 2014(2):57-60.
【16】孔浩辉,程志颖,张心颖.烟草中蛋白质含量的快速测定[J].烟草科技, 2014(3):38-41.
【17】张杰,马雁军,石睿,等.硫氰化钾与DCIC反应法测定烟草总植物碱[J].烟草科技, 2014(5):60-63.
【18】王洪波,郭军伟,殷延齐,等.卷烟侧流烟气中氨释放量的连续流动法测定[J].烟草科技, 2016(5):38-44.
【19】GB/T 14454.14-2008香料标准溶液、试液和指示液的制备[S].
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