Effect of Spark Plasma Sintering Temperature on Microstructure andMechanical Properties of Ti-45Al-6Nb-0.3W Alloy
摘 要
在不同温度下(1 150,1 200,1 250 ℃)对氩气雾化Ti-45Al-6Nb-0.3W合金粉末进行放电等离子烧结,研究了烧结温度对合金显微组织和力学性能的影响。结果表明:放电等离子烧结合金由γ相和α2相组成,随烧结温度升高,组织形态由片层和等轴状转变为全片层状,同时晶粒尺寸增大,γ相含量增加;合金密度随烧结温度升高略有增加,硬度变化不大;不同温度烧结合金的压缩性能均优于铸态合金的,1 200 ℃下烧结合金的室温压缩性能最好,抗压强度、压缩率分别为3 012 MPa,40.8%。
Abstract
Spark plasma sintering of argon atomized Ti-45Al-6Nb-0.3W alloy powders was carried out at different temperatures (1 150, 1 200, 1 250 ℃). The effect of sintering temperature on microstructure and mechanical properties of the alloy was studied. The results show that the spark plasma sintered TiAl alloy consisted of γ and α2 phases. With increasing sintering temperature, the structure morphology changed from lamellar and equiaxed shape to full lamellar shape, and the grain size and the γ phase content increased. The density of the alloy increased slightly with the sintering temperature, and the hardness changed little. The compression properties of the alloys sintered at different temperatures were better than those of the as-cast alloy. The alloy sintered at 1 200 ℃ showed the best room temperature compression performance with compressive strength of 3 012 MPa and compressibility of 40.8%.
中图分类号 T146.2 DOI 10.11973/jxgccl202006007
所属栏目 试验研究
基金项目 国家自然科学基金资助项目(51301157;51434007)
收稿日期 2019/5/6
修改稿日期 2020/4/26
网络出版日期
作者单位点击查看
备注杨冬野(1981-),男,上海人,讲师,博士
引用该论文: YANG Dongye,TIAN Wenqi,LI Jiuxiao,GU Xu,LIU Na,ZHANG Guoqing,SUN Jianfei. Effect of Spark Plasma Sintering Temperature on Microstructure andMechanical Properties of Ti-45Al-6Nb-0.3W Alloy[J]. Materials for mechancial engineering, 2020, 44(6): 28~32
杨冬野,田文琦,李九霄,谷旭,刘娜,张国庆,孙剑飞. 放电等离子烧结温度对Ti-45Al-6Nb-0.3W合金显微组织和力学性能的影响[J]. 机械工程材料, 2020, 44(6): 28~32
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参考文献
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【3】WU X H.Review of alloy and process development of TiAl alloys[J].Intermetallics, 2006,14(10/11):1114-1122.
【4】TRZASKA Z,COURET A,MONCHOUX J P.Spark plasma sintering mechanisms at the necks between TiAl powder particles[J].Acta Materialia, 2016,118:100-108.
【5】HUANG Y J,WANG Y,FAN H B,et al.A TiAl based alloy with excellent mechanical performance prepared by gas atomization and spark plasma sintering[J].Intermetallics, 2012,31:202-207.
【6】WANG Y,ZHANG C,LIU Y,et al.Microstructure characterization and mechanical properties of TiAl-based alloys prepared by mechanical milling and spark plasma sintering[J].Materials Characterization, 2017,128:75-84.
【7】陈华, 薛涛. 放电等离子烧结的钛铝合金组织及氧化性能研究[J]. 材料热处理学报, 2008, 29(1): 58-61.
【8】ZHOU H T,SU Y J,LIU N,et al.Modification of microstructure and properties of Ti-47Al-2Cr-4Nb-0.3W alloys fabricated by SPS with trace multilayer graphene addition[J].Materials Characterization, 2018,138:1-10.
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【10】LIU X W,ZHANG Z L,SUN R,et al.Microstructure and mechanical properties of beta TiAl alloys elaborated by spark plasma sintering[J].Intermetallics, 2014,55:177-183.
【11】TOBALDI D M,PULLAR R C,SEABRA M P,et al.Fully quantitative X-ray characterisation of Evonik Aeroxide TiO2 P25®[J].Materials Letters,2014,122:345-347.
【12】柴丽华.快速凝固TiAl基合金的组织演变研究[D].哈尔滨:哈尔滨工业大学,2010:68-79
【13】CHEN Y Y,YU H B,ZHANG D L,et al.Effect of spark plasma sintering temperature on microstructure and mechanical properties of an ultrafine grained TiAl intermetallic alloy[J].Materials Science and Engineering:A, 2009,525(1/2):166-173.
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