水体中合成麝香检测方法的研究进展
Research Progress on Detection Methods for Synthetic Musk in Water Body
摘 要
合成麝香被广泛应用于个人护理产品和生活用品中,在环境中的污染程度呈逐年上升的趋势,准确测定环境中合成麝香的含量具有重要意义。综述了水体中合成麝香的前处理方法(包括固相萃取法、固相微萃取法、液液萃取法、液液微萃取法、索氏提取法、超声辅助提取法、加速溶剂萃取法和QuEChERS等)和仪器分析方法(包括气相色谱-质谱法、气相色谱-串联质谱法、高效液相色谱法、液相色谱-串联质谱法和新型荧光光谱法等),并对相关研究领域的发展趋势进行了展望(引用文献52篇)。
水体
前处理方法
仪器分析方法
研究进展
synthetic musk
water body
pretreatment method
instrumental analysis method
research progress
Abstract
Synthetic musk was widely used in personal care products and daily necessities, and the pollution level in the environment was increasing with years. It was of great significance to accurately determine synthetic musk in the environment. The pretreatment methods (including solid phase extraction, solid phase micro-extraction, liquid-liquid extraction, liquid-liquid micro-extraction, Soxhlet extraction, ultrasound-assisted extraction, accelerated solvent extraction and QuEChERS) and instrumental analysis methods (including gas chromatography-mass spectrometry, gas chromatography-tandem mass spectrometry, high performance liquid chromatography, liquid chromatography-tandem mass spectrometry and new fluorescence spectrophotometry) of synthetic musk in water body were reviewed, and the development trend of relevant research field was prospected (52 ref. cited).
中图分类号 O65 DOI 10.11973/lhjy-hx202305021
所属栏目 专题报道(色谱-质谱联用技术在新型污染物分析中的应用)
基金项目 国家自然科学基金(22206110),山东省自然科学基金(ZR2022QB072、ZR2022QD038)
收稿日期 2023/2/13
修改稿日期
网络出版日期
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备注刁子珊,硕士研究生,主要从事新污染物环境分析与监测相关研究
引用该论文: DIAO Zishan,CHEN Weidong,MA Hui,XIE Xiaomin,LI Yun,ZHANG Xiaohan. Research Progress on Detection Methods for Synthetic Musk in Water Body[J]. Physical Testing and Chemical Analysis part B:Chemical Analysis, 2023, 59(5): 612～620
刁子珊,陈卫东,马慧,解晓敏,李赟,张晓寒. 水体中合成麝香检测方法的研究进展[J]. 理化检验－化学分册, 2023, 59(5): 612～620
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参考文献
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【2】MARCHAL M, BELTRAN J. Determination of synthetic musk fragrances[J]. International Journal of Environmental Analytical Chemistry, 2016,96(13):1213-1246.
【3】佟玲,田芹,潘萌,等.环境中合成麝香类化合物残留现状及其分析方法研究进展[J].生态学杂志, 2017,36(5):1426-1435.
【4】高艳蓬,李桂英,马盛韬,等.合成麝香的研究新进展与当前挑战:从人体护理、环境污染到人体健康[J].化学进展, 2017,29(9):1082-1092.
【5】HOMEM V, SILVA E, ALVES A, et al. Scented traces-dermal exposure of synthetic musk fragrances in personal care products and environmental input assessment[J]. Chemosphere, 2015,139:276-287.
【6】ABEDI G, TALEBPOUR Z, JAMECHENARBOO F. The survey of analytical methods for sample preparation and analysis of fragrances in cosmetics and personal care products[J]. Trends in Analytical Chemistry, 2018,102:41-59.
【7】LIU J N, ZHANG W Y, ZHOU Q X, et al. Polycyclic musks in the environment:A review of their concentrations and distribution, ecological effects and behavior, current concerns and future prospects[J]. Critical Reviews in Environmental Science and Technology, 2021,51(4):323-377.
【8】ARRUDA V, SIMÕES M, GOMES I B. Synthetic musk fragrances in water systems and their impact on microbial communities[J]. Water, 2022,14(5):692-708.
【9】CUNHA S C, TRABALÓN L, JACOBS S, et al. UV-filters and musk fragrances in seafood commercialized in Europe Union:Occurrence, risk and exposure assessment[J]. Environmental Research, 2018,161:399-408.
【10】KATURI G P, FAN X H, SIDDIQUE S, et al. A selective and sensitive gas chromatography-tandem mass spectrometry method for quantitation of synthetic musks in human serum[J]. Journal of AOAC International, 2020,103(6):1461-1468.
【11】DING T D, LI W, CAI M, et al. Algal toxicity, accumulation and metabolic pathways of galaxolide[J]. Journal of Hazardous Materials, 2020,384:121360.
【12】PAROLINI M, MAGNI S, TRAVERSI I, et al. Environmentally relevant concentrations of galaxolide (HHCB) and tonalide (AHTN) induced oxidative and genetic damage in Dreissena polymorpha[J]. Journal of Hazardous Materials, 2015,285:1-10.
【13】BLAHOVA J, DIVISOVA L, PLHALOVA L, et al. Multibiomarker responses of juvenile stages of zebrafish (Danio rerio) to subchronic exposure to polycyclic musk tonalide[J]. Archives of Environmental Contamination and Toxicology, 2018,74(4):568-576.
【14】LI X X, HE W, ZHAO Y Y, et al. Dermal exposure to synthetic musks:Human health risk assessment, mechanism, and control strategy[J]. Ecotoxicology and Environmental Safety, 2022,236:113463.
【15】TUMOVÁ J, ŠAUER P, GOLOVKO O, et al. Effect of polycyclic musk compounds on aquatic organisms:A critical literature review supplemented by own data[J]. Science of the Total Environment, 2019,651:2235-2246.
【16】国家市场监督管理总局,国家标准化管理委员会.化妆品中人工合成麝香的测定 气相色谱-质谱法:GB/T 40844-2021[S].北京:中国标准出版社, 2021.
【17】刘洪涛,梁少霞,李梦婷,等.人工合成麝香的分析方法及环境污染现状[J].分析测试学报, 2017,36(12):1526-1535.
【18】吴春英,白鹭,陆文龙,等.气相色谱-串联质谱法同时快速检测环境水样中11种合成麝香[J].分析科学学报, 2016,32(2):188-192.
【19】LOPEZ-NOGUEROLES M, LORDEL-MADELEI-NE S, CHISVERT A, et al. Development of a selective solid phase extraction method for nitro musk compounds in environmental waters using a molecularly imprinted sorbent[J]. Talanta, 2013,110:128-134.
【20】MAIDATSI K V, CHATZIMITAKOS T G, SAKKAS V A, et al. Octyl-modified magnetic graphene as a sorbent for the extraction and simultaneous determination of fragrance allergens, musks, and phthalates in aqueous samples by gas chromatography with mass spectrometry[J]. Journal of Separation Science, 2015,38(21):3758-3765.
【21】FAN Y F, JIANG H L, CHEN X F, et al. Room-temperature synthesis of nitrogen-rich conjugated microporous polymers for solid-phase extraction of trace synthetic musks[J]. Food Chemistry, 2023,404:134681.
【22】CELEIRO M, LAMAS J P, VILA M, et al. Determination of multiclass personal care products in continental waters by solid-phase microextraction followed by gas chromatography-tandem mass spectrometry[J]. Journal of Chromatography A, 2019,1607:460398.
【23】GONZÁLEZ-HERNÁNDEZ P, PACHECOFERN-ÁNDEZ I, BERNARDO F, et al. Headspace solid-phase microextraction based on the metal-organic framework CIM-80(Al) coating to determine volatile methylsiloxanes and musk fragrances in water samples using gas chromatography and mass spectrometry[J]. Talanta, 2021,232:122440.
【24】GRAU J, BENEDÉ J L, CHISVERT A. Polydopamine-coated magnetic nanoparticles for the determination of nitro musks in environmental water samples by stir bar sorptive-dispersive microextraction[J]. Talanta, 2021,231:122375.
【25】VALLECILLOS L, BORRULL F, SANCHEZ J M, et al. Sorbent-packed needle microextraction trap for synthetic musks determination in wastewater samples[J]. Talanta, 2015,132:548-556.
【26】JO J, LEE J Y, LEE H E, et al. Determination of twelve synthetic musk compounds in estuary and coastal areas near Han River of Korea by improved liquid-liquid extraction coupled with GC/MS[J]. International Journal of Environmental Analytical Chemistry, 2021:1-12.
【27】VIMALKUMAR K, NIKHIL N P, ARUN E, et al. Synthetic musks in surface water and fish from the rivers in India:Seasonal distribution and toxicological risk assessment[J]. Journal of Hazardous Materials, 2021,414:125558.
【28】CUNHA S C, FERREIRA R, MARMELO I, et al. Occurrence and seasonal variation of several endocrine disruptor compounds (pesticides, bisphenols, musks and UV-filters) in water and sediments from the estuaries of Tagus and Douro Rivers (NE Atlantic Ocean coast)[J]. The Science of the Total Environment, 2022,838(2):155814.
【29】HOMEM V, ALVES A, ALVES A, et al. Ultrasound-assisted dispersive liquid-liquid microextraction for the determination of synthetic musk fragrances in aqueous matrices by gas chromatography-mass spectrometry[J]. Talanta, 2016,148:84-93.
【30】佟玲,田芹,杨志鹏,等.沉积物中14种典型人工合成麝香加速溶剂萃取-气相色谱-串联质谱快速分析方法研究[J].岩矿测试, 2020,39(4):587-596.
【31】王梓,杨兆光,李海普.超声辅助提取-固相萃取-气相色谱-质谱法测定污泥中12种多环芳烃[J].理化检验-化学分册, 2020,56(2):172-178.
【32】董小锋,楼迎华,刘晓文,等.北戴河湿地沉积物中人工合成麝香分布特征与环境风险评估[J].环境化学, 2019,38(3):662-668.
【33】TASSELLI S, GUZZELLA L. Polycyclic musk fragrances (PMFs) in wastewater and activated sludge:Analytical protocol and application to a real case study[J]. Environmental Science and Pollution Research, 2020,27(25):30977-30986.
【34】ZHANG H D, BU Q W, WU D K, et al. Polycyclic musks in surface water and sediments from an urban catchment in the megacity Beijing, China[J]. Environmental Pollution, 2020,263:114548.
【35】PINTADO-HERRERA M G, GONZÁLEZ-MAZO E, LARA-MARTÍN P A. In-cell clean-up pressurized liquid extraction and gas chromatography-tandem mass spectrometry determination of hydrophobic persistent and emerging organic pollutants in coastal sediments[J]. Journal of Chromatography A, 2016,1429:107-118.
【36】SARRAF M, BEIG-BABAEI A, NAJI-TABASI S. Application of QuEChERS method for extraction of functional compounds[J]. SN Applied Sciences, 2020,2(11):1858.
【37】RAMOS S, HOMEM V, SANTOS L. Development and optimization of a QuEChERS-GC-MS/MS methodology to analyse ultraviolet-filters and synthetic musks in sewage sludge[J]. Science of the Total Environment, 2019,651:2606-2614.
【38】ZHANG H, BAYEN S, KELLY B C. Multi-residue analysis of legacy POPs and emerging organic contaminants in Singapore's coastal waters using gas chromatography-triple quadrupole tandem mass spectrometry[J]. Science of the Total Environment, 2015,523:219-232.
【39】CHUNG W H, TZING S H, DING W H. Dispersive micro solid-phase extraction for the rapid analysis of synthetic polycyclic musks using thermal desorption gas chromatography-mass spectrometry[J]. Journal of Chromatography A, 2013,1307:34-40.
【40】GODAYOL A, BESAL AU'G E, ANTICÓ E, et al. Monitoring of sixteen fragrance allergens and two polycyclic musks in wastewater treatment plants by solid phase microextraction coupled to gas chromatography[J]. Chemosphere, 2015,119:363-370.
【41】佟玲,潘萌,杨志鹏,等.搅拌棒萃取-气相色谱-质谱法分析地表水中合成麝香及紫外线吸收剂[J].质谱学报, 2019,40(3):233-243.
【42】CAVALHEIRO J, PRIETO A, MONPERRUS M, et al. Determination of polycyclic and nitro musks in environmental water samples by means of microextraction by packed sorbents coupled to large volume injection-gas chromatography-mass spectrometry analysis[J]. Analytica Chimica Acta, 2013,773:68-75.
【43】TASSELLI S, VALENTI E, GUZZELLA L. Polycyclic musk fragrance (PMF) removal, adsorption and biodegradation in a conventional activated sludge wastewater treatment plant in Northern Italy[J]. Environmental Science and Pollution Research, 2021,28(28):38054-38064.
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