- 中国学术期刊(光盘版)全文收录期刊
- 中国学术期刊综合评价数据库来源期刊
- 中国期刊网、万方数据库入编期刊
- 中文科技期刊数据库(全文版)收录期刊
- 中国期刊全文数据库全文收录期刊
- 中国机械工程学会 理化检验分会 失效分析分会 会刊
| Citation: |
GAO Qianwen, LI Yixue, FENG Dan, SHI Xuefang. Preparation of transmission electron microscopy microcolumn samples based on focused ion beam-scanning electron microscopy[J]. PHYSICAL TESTING AND CHEMICAL ANALYSIS PART A:PHYSICAL TESTING, 2024, 60(9): 30-33. DOI: 10.11973/lhjy-wl240170
|
By using focused ion beam-scanning electron microscopy to improve the traditional method of transmission electron microscopy sample preparation. By changing the area and effect of ion beam assisted deposition, and improving the U-shaped cut to L-shaped cut, the compressed mouse bone micro-pillars samples were successfully extracted onto a dedicated copper mesh. The extracted sample could be precisely thinned by ion beam, and the direction of collagen fibers could be observed under transmission electron microscopy.
| [1] |
田琳,付琴琴,单智伟 ．聚焦离子束在微纳尺度材料力学性能研究中的应用[J]．中国材料进展,2013,32(12)：706-715．
|
| [2] |
周伟敏 ．高性能聚焦离子束技术的应用[J]．理化检验(物理分册),2004,40(9)：453-456．
|
| [3] |
李怡雪,丁莹,张国栋,等 ．一种基于聚焦离子束的石英玻璃平面透射电镜试样制备方法[J]．理化检验(物理分册),2023,59(1)：27-30．
|
| [4] |
KIM T H ,KANG M C ,JUNG G B ,et al ．Novel method for preparing transmission electron microscopy samples of micrometer-sized powder particles by using focused ion beam[J]．Microscopy and Microanalysis,2017,23(5)：1055-1060．
|
| [5] |
LIU T ,JIN H Y ,XU L L ,et al ．Transmission electron microscopy sample preparation method for micrometer-sized powder particles using focused ion beam[J]．Micron,2021,143：103030．
|
Supported by: Beijing Renhe Information Technology Co., Ltd. 
DownLoad: